Effects of Sintering Process on the Properties of Ti3SiC2/Cu Composite

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In this paper, a new type of Ti3SiC2/Cu composites with the volume fractions of 30% Ti3SiC2 particle was prepared by hot pressing and vacuum sintering respectively. The effects of sintering temperature and holding time on the density, resistance and Vickers hardness of Cu-30vol%Ti3SiC2 composite were investigated. The results show that the mechanical properties of the composites prepared by hot pressing are better than that prepared by vacuum sintering. The relative densities of Cu-30vol% Ti3SiC2 composites are rather high in suitable sintering conditions. It achieved 100% for the composites prepared by hot pressing at 930°C for 2h, and 98.4% for the composites prepared by vacuum sintering at 1250°C for 1h. At the same time, the maximum Vickers hardness reached 1735MPa at 900°C by hot pressing. The resistance and Vickers hardness of the composites decreased with an increase in sintering temperature, whereas the density increased. Scanning electron microscope (SEM) and energy-dispersive spectroscopy (EDS) were used to observe the microstructure of the composites. The relationship between microstructure and mechanical properties was discussed.

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Key Engineering Materials (Volumes 512-515)

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377-381

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June 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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[1] S.Y. Zhang, F.Q. Meng, Y.Y. Chen, Q.C.Li, Research Progress of Metal Matrix Composites Reinforced with Particles, Materials Review.1999, NO.2, 66-71.

Google Scholar

[2] K. Han, J.D. Embury, J.R. Sims, et al., The fabrication, properties and microstructure of Cu–Ag and Cu–Nb composite conductors, Mater. Sci. Eng., A. 267 (1999) 99-114.

DOI: 10.1016/s0921-5093(99)00025-8

Google Scholar

[3] M.W. Barsoum, T.El-Raghy, Synthesis and Characterization of a Remarkable Ceramic: Ti3SiC2, J. Am. Ceram. Soc. 79(1996) 1953.

Google Scholar

[4] Z.F. Zhang, Z.M. Sun, H. Hashimoto, T. Abe, Application of pulse discharge sintering (PDS) technique to rapid synthesis of Ti3SiC2 from Ti/Si/C powders, J. Eur. Ceram. Soc. 22 (2002) 2957.

DOI: 10.1016/s0955-2219(02)00044-4

Google Scholar

[5] B.J. Kooi, R.J. Poppen, N.J.M. Carvalho, et al., Ti3SiC2: A damage tolerant ceramic studied with nano-indentations and transmission electron microscopy, Acta Mater.. 51 (2003) 2859.

DOI: 10.1016/s1359-6454(03)00091-0

Google Scholar

[6] J.Zhang, J.Y. Wang, Y.C. Zhou. Structure stability of Ti3AlC2 in Cu and microstructure evolution of Cu–Ti3AlC2 composites, Acta Mater.. 55(2007)4381-4390.

DOI: 10.1016/j.actamat.2007.03.033

Google Scholar

[7] H.P. Guo, J.Zhang, F.Z.Li, J.J. Yin, Y.C. Zhou, Surface strengthening of Ti3SiC2 through magnetron sputtering Cu and subsequent annealing, J. Eur. Ceram. Soc.. 28(2008)2099-2107.

DOI: 10.1016/j.jeurceramsoc.2008.02.011

Google Scholar

[8] J.J. Sun, Y.Zhou, J.R.Lu, S.B.Li, Z.Y. Huang, H.X. Zhai, Preparation and properties of Ti3SiC2/Cu composites, Mater. Sci. Eng. Powder Metallurgy. Aug.2011,Vol.16 No.4,587-590.

Google Scholar

[9] Y.C. Zhou, W.L.Gu, Chemical reaction and stability of Ti3SiC2 in Cu during high-temperature processing of Cu/Ti3SiC2 composites, Z. Metallkd., 95(1)50-56(2004).

Google Scholar