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Synthesis and Kinetic of Palladium Nanotube Using Polymer Compound

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Abstract:

The palladium nanotube was synthesized by template wetting and annealing process. And the activation energy for formation of the palladium metal from palladium acetate was evaluated. The activation energy was evaluated by Friedman method and the values were in the ranges between 65 and 98 kJ/mol. The diameters and lengths of synthesized palladium nanotubes ranged from 130 to 190 nm and from 2 to 3 μm, respectively. The palladium nanotubes can be successfully fabricated by the template wetting process, and the crystalline structure is confirmed by XRD. From DSC results the thermal decomposition of precursor containing palladium acetate/PLLA occurred at 248°C, which corresponds to the precipitation of palladium metal.

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Periodical:

Key Engineering Materials (Volume 543)

Pages:

137-140

DOI:

https://doi.org/10.4028/www.scientific.net/KEM.543.137

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Online since:

March 2013

Authors:

Jong Ho Lee, Choong Soo Chi, Han Jun Oh

Keywords:

Friedman Method, Nanotube, Palladium, Template Wetting

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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References

[1] E.C. Walter, F. Favier and R.M. Penner: Anal. Chem. Vol. 74 (2002), p.1546.

Google Scholar

[2] V. Mazumder and S. Sun: J. Am. Cem. Soc. Vol. 131 (2009), p.4588.

Google Scholar

[3] C. Xu, H. Wang, P.K. Shen and S.P. Jiang: Adv. Mater. Vol. 19 (2007), p.4256.

Google Scholar

[4] J. Ge, W. Xing, X. Xue, C. Liu, T. Lu and J. Liao: J. Phys. Chem. C Vol. 111 (2007), p.17305.

Google Scholar

[5] Y. Nishihata, J. Mizuki, T. Akao, H. Tanaka, M. Uenishi, M. Kimura, T. Okamoto and N. Hamada: Nature Vol. 418 (2002), p.164.

DOI: 10.1038/nature00893

Google Scholar

[6] C. R. Martin: Accounts Chem. Res. Vol. 28 (1995), p.61.

Google Scholar

[7] J. C. Hulteen and C. R. Martin: J. Mater. Chem. Vol. 7 (1997), p.1075.

Google Scholar

[8] M. Steinhart, R. B. Wehrspohn, U. Gösele and J. H. Wendorff: Angew. Chem. Int. Ed. Vol. 43 (2004), p.1334.

DOI: 10.1002/anie.200300614

Google Scholar

[9] Y. Luo, S. K. Lee, H. Hofmeister, M. Steinhart and U. Gösele, Nano Lett. Vol. 4 (2004), p.143.

Google Scholar

[10] V. Logvinenko , O. Polunina, Yu. Mikhailov, K. Mikhailov and B. Bokhonov: J. Therm. Anal. Calorim. Vol. 90 (2007), p.813.

DOI: 10.1007/s10973-006-7883-9

Google Scholar

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