Preparation and Ferroelectric Properties of BaTiO3 Nanotubes

Article Preview

Abstract:

BaTiO3 nanotube arrays are prepared by hydrothermal reaction using the TiO2 nantotubes prepared by anodic oxidation reaction. The element, structure, elementary composition and ferroelectric properties are researched by SEM, XRD and TF Analyzer. The result shows that the prepared BaTiO3 arranged orderly and have tetragonal structure after annealing. The diffracted intensity increased with the hydrothermal temperature rising up. With the increasing of Ba(OH)2 concentration, remnant polarization intensity and coercive field climbed up and then decreased. With the increasing of hydrothermal temperature, remnant polarization intensity and coercive field increased. When the Ba(OH)2 concentration is 0.3mol/L, the hydrothermal temperature is 260°C,the remnant polarization and coercive field of the samples reached the maximum and respectively reached 6.69mC/cm2 and 1.32 kV/cm.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

159-163

Citation:

Online since:

July 2015

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2015 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] S. Iijima, Helical microtubules of graphitic carbon, J. Nature. 354(1991) 56-58.

DOI: 10.1038/354056a0

Google Scholar

[2] Florentina Maxim, Paula Ferreira, Paula M. Vilarinho, Ian Reaney, Hydrothermal Synthesis and Crystal Growth Studies of BaTiO3 Using Ti Nanotube Precursors, J. 9(2008) 3309-3315.

DOI: 10.1021/cg800215r

Google Scholar

[3] Zhang Haitao, Deng Xiangyun, Chen Xin, Low temperature hydrothermal synthesis and performances of nanotube patterned barium titanates thin films, J. 42(2011) 271-275.

Google Scholar

[4] Y. N, Xia, J, A. Rogers, G. M. Whitesides, et al, Unconventional methods for fabricating md patterning nanostructures, J. Chem. Rev. 7(1999) 1823-1848.

DOI: 10.1021/cr980002q

Google Scholar

[5] Gao Daojiang, Xiao Dingquan, Zhang Wen, Hydrothermal-electrochemical technology and it's applications for preparing of ceramic thin films, J. Journal of Function Materials. 33(2002) 240-245.

Google Scholar

[6] Padture Nitin P., Wei Xuezheng, Hydrothermal Synthesis of Thin Films of BaTiO3 Ceramic Nano - Tubes at 200°C,J. Journal of the American Ceramic Society. 86(2004) 2215-2217.

DOI: 10.1111/j.1151-2916.2003.tb03636.x

Google Scholar

[7] Mao Yuanbing, Banerjee Sarbajit, Wong Stanislaus S, Hydrothermal synthesis of perovskite nanotubes, J. Chemical Communications. 3(2003) 408-409.

Google Scholar