Mechanical Properties of Hydroxyapatite Ceramic Prepared from Micropowder and Nanopowder

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In this work, hydroxyapatite ceramics were prepared from hydroxyapatite micropowder and nanopowder. The hydroxyapatite nanopowder was obtained from natural buffalo bone by using a high speed vibro-milling machine for 2 hour. The green compacted pellets of all HA powders were subsequently sintered at 1200, 1250, 1300 and 1350°C for 3 hour and then the physical and mechanical characterizations as well as microstructural evaluation have been carried out. It was found that the optimum sintering temperature were 1250°C by fabricated from nanopowder which gave the HA nanoceramic with the maximum bending strength of 78.6±2.6 MPa. This is about 200% higher than that of the sample which fabricated from HA micropowder.

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Materials Science Forum (Volume 1074)

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17-22

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November 2022

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© 2022 Trans Tech Publications Ltd. All Rights Reserved

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[1] K A. Hing, Bone repair in the twenty-first century: Biology, chemistry or engineering, Phil. Trans. R. Soc. Lond. (2004) 2821–2850.

Google Scholar

[2] W Suchanek, M Yashima, M Kakihana, M Yashimura, Hydroxyapatite ceramics with selected sintering additives, Biomaterials 18 (1997) 923-933.

DOI: 10.1016/s0142-9612(97)00019-7

Google Scholar

[3] F N Oktar, G Gultekin, Sintering effects on mechanical properties of glass-reinforced hydroxyapatite composites, Ceramics International 28 (2002) 617-621.

DOI: 10.1016/s0272-8842(02)00017-2

Google Scholar

[4] S J Katita, S Bose, H L Hosick, A Bandyopadhyay, CaO – P2O5 –Na2O-based sintering additives for hydroxyapatita ( HAp) ceramics, Biomaterials 25 (2004) 2331-9.

DOI: 10.1016/j.biomaterials.2003.09.012

Google Scholar

[5] J C Knowles, S Talal, J D Santos, Sintering effects in a glass reinforced hydroxyl apatite, Biomaterials 17 (1996) 1437-1442.

DOI: 10.1016/0142-9612(96)87287-5

Google Scholar

[6] T Sleboda, K Muszka, J Majta, P Hale, R N J Wright, The possibilities of mechanical property control in fine grained structures, J Mater Process Tech (2006) 461-464.

DOI: 10.1016/j.jmatprotec.2006.03.202

Google Scholar

[7] M A Meyers, A Mishra, D J Benson, Mechanical Properties of Nanocrystalline Materials, Progress in Mater Sci 51 (2006) 427-556.

DOI: 10.1016/j.pmatsci.2005.08.003

Google Scholar

[8] S J Kalita, H A Bhatt, Nanocrystalline Hydroxyapatite Doped with Magnesium and Zinc: Synthesis and Characterization, Mater Sci Eng C 27 (2007) 837-848.

DOI: 10.1016/j.msec.2006.09.036

Google Scholar

[9] G Dewith, H H M Wagemans, Ball-on-ring test revisited, J Amer Ceram Soc 72(8) (1989) 1538-1541.

Google Scholar

[10] T Kokubo, H.M Kim, M Kawashita, Novel bioactive materials with different mechanical properties, Biomaterials 24 (2003) 2161-2175.

DOI: 10.1016/s0142-9612(03)00044-9

Google Scholar

[11] G Geogiou, J C Knowles, Glass reinforced hydroxyapatite for hard tissue surgery – Part1 Mechanic properties, Biomaterials 22 (2001) 2811-2815.

DOI: 10.1016/s0142-9612(01)00025-4

Google Scholar