Preparation of Lanthanum Oxide Nanoparticles by Chemical Precipitation Method

Article Preview

Abstract:

This paper investigated synthesis of Lanthanum oxide nanoparticles by precipitation method. Effects of reactant concentration, precipitator and dispersant agent on properties of Lanthanum oxide particles were studied. Lanthanum oxide particles were characterized by XRD and SEM. Experimental results showed that ammonium bicarbonate and PEG20000 were appropriate precipitation and dispersant respectively. The optimum process conditions were as follows: concentration of Lanthanum nitrate was 0.18mol/L, concentration ammonium bicarbonate of was 0.6mol/L, reaction temperature was 30. The average particles size of Lanthanum oxide powders with spherical shape gained was about 188 nm.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

233-236

Citation:

Online since:

June 2012

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2012 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] CHEN Hai-song, YU Li-xin, XU Hai-sheng, et al. Marco-kinetics of propane dehydrogenation on Cr-Al catalyst improved by rare-earth aids [J]. J Chem Eng of Chinese Univ, 1999, 13(1): 38-43.

Google Scholar

[2] CHEN Zhan-heng. Rare earth new materials and their application in the field of high technology [J]. Chinese Rare Earths, 2000, 21(1): 53-57.

Google Scholar

[3] Tamai H, Ikeya T, Nishiyama F, et al. NO decomposition by ultrafine noble metals dispersed on the rare earth phosphate hollow particles [J]. Journal of Materials Science, 2000, (35): 4945-4953.

Google Scholar

[4] Weber J K, Richard, Abadie, Johan G, et al. Single phase rare earth oxide-aluminum oxide glasses [P]. US 6482458, 2002, 11-19.

Google Scholar

[5] McCauley J R, McDaniel J G. Catalyst and process for preparing and using same [P]. USP 6, 117, 813, (2000).

Google Scholar

[6] Bianco, Robert, Buckman, et al. Oxide strengthened molybdenum-rhenium alloy [P]. USP 6, 102, 979, (2000).

Google Scholar

[7] ZHANG Ji-guang, MA Lin, XU Yan. The preparation and characterization of ultrafine Lanthanum oxide by sol-gel process [J]. Journal of Fudan University(Natural Science), 1999, 38(1): 24-28.

Google Scholar

[8] ZHANG Mei, YANG Xu-jie, LU Lu-de, WANG Xin. Preparation and characterization of La2O3 nanocrystals [J]. Aerospace Materials & Technology, 1999, (5): 38-40.

Google Scholar

[9] YAO Chao, MA Jiang-quan, LIN Xi-ping. The preparation of nanometer lanthanide oxide. Journal of Chemical Engineering of Chinese Universities, 2003, 17( 6) : 685- 688.

Google Scholar