Paper Titles
Microstructures and Mechanical Properties of Two-Phase FeNiMnAl Alloys
p.2549
Effect of Warm-Rolling on the Formation of Microstructure and Microtexture of the Constituent Phases in a Duplex Steel
p.2555
Identification of Crystal Structure and Crystallographic Features of NiMnGa Thin Films by Combination of X-Ray Diffraction (XRD) and Electron Backscatter Diffraction (EBSD)
p.2561
Influence of Strain Path on Work Hardening and Texture in an Austenitic Stainless Steel
p.2567
Formation of Multiple Twinned Structural Units in Electrodeposited Nickel after Annealing
p.2573
Influence of New System Nano-Inhibitors on the Abnormal Grain Growth with Goss Crystallographic Orientation of Silicon Steels
p.2579
Disorientation Relations during the Early Stages of Recrystallization in Medium and Low SFE fcc Metals
p.2585
Effect of the Channel Angle of One-Pass ECAP Prior to Cold Rolling on the Microstructure and Texture of Metallic Sheets
p.2591
Deformation Texture and Microstructure Evolution in Nickel and Nickel-Cobalt Alloys
p.2597

Formation of Multiple Twinned Structural Units in Electrodeposited Nickel after Annealing

Article Preview

Abstract:

Electrodeposition is an advanced synthesis technique which involves the creation of a coating or free-standing material through an electrolytic process. Organic additives such as saccharin have been frequently used in electroplating operations to moderate deposit growth rates and to control film quality. In the present study, plating of Nickel without additives has resulted in a sub-microcrystalline microstructure and a <110>-fibre texture in growth direction. Structural units in form of groups of grains possessing a common <110>-zone axis in growth direction and low-Σ relationships between them have been found in the microstructure by use of EBSD. Upon annealing, grain growth sets in. However, the structural units and the texture are preserved up to 550°C. This means that the structural units stabilize the microstructure; there is no orientation change when grain growth occurs (e.g. by twinning). The low-Σ boundaries of the structural units are described in detail and texture development upon annealing is discussed in connection with results from previous studies on Ni and Ni-alloys of different initial texture.

You might also be interested in these eBooks
THERMEC 2013 View Preview

Info:

Periodical:

Materials Science Forum (Volumes 783-786)

Pages:

2573-2578

DOI:

https://doi.org/10.4028/www.scientific.net/MSF.783-786.2573

Citation:

Cite this paper

Online since:

May 2014

Authors:

Alexander Kahrimanidis*, Uta Klement

Keywords:

5-Fold Symmetry, EBSD, Electrodeposition, Grain Growth, Nickel, Structural Unit, Texture, Twin Boundaries, Σ-Grain Boundaries

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

References

[1] C.S. Lin, P.C. Hsu, L. Chang, C.H. Chen, J. Appl. Electrochem., 31 (2001) 925-933.

Google Scholar

[2] I. Kim, S.G. Lee, Texture Microstruct., 34 (2000) 159-169.

Google Scholar

[3] C.B. Nielsen, A. Horsewell, J. Appl. Electrochem., 27 (1997) 839-845.

Google Scholar

[4] J. Amblard, I. Epelboin, M. Froment, G. Maurin, J. Appl. Electrochem., 9 (1979) 233-242.

DOI: 10.1007/bf00616093

Google Scholar

[5] G. Lucadamo, D.L. Medlin, N.Y.C. Yang, J.J. Kelly, A.A. Talin, Phil. Mag., 85 (2005) 2549-2560.

Google Scholar

[6] G.M. Janowski, G.R. Stafford, Metall. Mater. Trans. A, 23A (1992) 2715-2723.

Google Scholar

[7] B.Y.C. Wu, P.J. Ferreira, C.A. Schuh, Metall. Mater. Trans. A, 36A (2005) 1927-(1936).

Google Scholar

[8] T. Watanabe, S. Tsurekawa, Acta Mater., 47 (1999) 4171-4185.

Google Scholar

[9] L. Lu, Y. Shen, X. Chen, L. Qian, K. Lu, Science, 304 (2004) 422-426.

Google Scholar

[10] I.S. Yasnikov, A.A. Vikarchuk, D.A. Denisova, N.N. Gryzunova, I.I. Tsybuskina, Tech. Phys+, 52 (2007) 1328-1331.

DOI: 10.1134/s106378420710012x

Google Scholar

[11] V.G. Gryaznov, J. Heydenreich, A.M. Kaprelov, S.A. Nepijko, A.E. Romanov, J. Urban, Cryst. Res. Technol., 34 (1999) 1091-1119.

DOI: 10.1002/(sici)1521-4079(199911)34:9<1091::aid-crat1091>3.0.co;2-s

Google Scholar

[12] Y.T. Zhu, X.Z. Liao, R.Z. Valiev, Appl. Phys. Letters, 86 (2005) 103112.

Google Scholar

[13] E.M. Bringa, D. Farkas, A. Caro, Y.M. Wang, J. McNaney, R. Smith, Scripta Mater., 59 (2008) 1267-1270.

DOI: 10.1016/j.scriptamat.2008.08.041

Google Scholar

[14] P. Huang, G.Q. Dai, F. Wang, K.W. Xu, Y.H. Li, Appl. Phys. Letters, 95 (2009) 203101.

Google Scholar

[15] V. Yamakov, D. Wolf, S.R. Phillpot, H. Gleiter, Acta Mater., 50 (2002) 5005-5020.

Google Scholar

[16] U. Klement, C. Oikonomou, R. Chulist, B. Beausir, L. Hollang, W. Skrotzki, Mater. Sci. Forum, 702-703 (2012) 928-931.

DOI: 10.4028/www.scientific.net/msf.702-703.928

Google Scholar

[17] H. Rösner, C. Kübel, Y. Ivanisenko, L. Kurmanaeva, S.V. Divinski, M. Peterlechner, G. Wilde, Acta Mater., 59 (2011) 7380-7387.

DOI: 10.1016/j.actamat.2011.08.020

Google Scholar

[18] M.L. Kronberg, F.H. Wilson, Trans. Am. Inst. Min. Metall. Eng., 185 (1949) 501-514.

Google Scholar

[19] D.G. Brandon, Acta Metall., 14 (1966) 1479-1484.

Google Scholar

[20] V.Y. Gertsman, K. Tangri, Scripta Metall. Mater., 32 (1995) 1649-1652.

Google Scholar

[21] D. J. Evans, The structure of nickel electrodeposits in relation to some physical properties, Trans. Faraday Soc. 54 (1958) 1086.

DOI: 10.1039/tf9585401086

Google Scholar

[22] U. Klement, M. da Silva, W. Skrotzki, J. Microscopy 230 (2008) 455-463.

Google Scholar

[23] U. Klement, U. Erb, A.M. El-Sherik, K.T. Aust, Mat. Sci. Eng. A 203 (1995) 177-186.

Google Scholar

[24] F. Czerwinski, J.A. Szpunar, Nanostr. Materials 11 (1999) 669-676.

Google Scholar

[25] A.A. Rasmussen, A. Gholina, P. Trimby, M.A.J. Somers, Mater. Sci. Forum 467-470 (2004) 1345-1350.

Google Scholar