Microstructure and Mechanical Properties of 6013 Aluminium Alloy Processed by a Combination of ECAP and Preaging Treatment

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Microstructure and mechanical properties of a 6013 Al-Mg-Si-Cu aluminum alloy processed by a combination of equal channel angular pressing (ECAP) and preaging treatment were comparatively investigated using quantitative X-ray diffraction (XRD) measurements, transmission electron microscopy (TEM) and tensile tests. In addition, the precipitation sequences were obtained by thermodynamic calculations using the FactSage software package. Average grain sizes measured by XRD are in the range 211–501 nm while the average dislocation density is in the range 0.35-1.0 × 1014 m-2 in the deformed alloy. TEM analysis reveals that fine needle β′′ precipitates with an average length of 4-10 nm are uniformly dispersed in the preaging ECAPed alloy. The local dislocation density in this sample is as high as 2.2×1017 m-2. The strength is significantly increased in the preaging-ECAPed samples as compared to that of the undeformed counterparts. The highest yield strength among the preaging ECAPed alloys is 322 MPa. This value is about 1.25 times higher than that (258 MPa) of the static peak-aging sample. The high strength in the preaging ECAPed alloy is suggested to be related to grain size strengthening and dislocation strengthening, as well as precipitation strengthening contributed from both preaging treatment and ECAP deformation.

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437-443

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November 2016

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© 2017 Trans Tech Publications Ltd. All Rights Reserved

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[1] R.Z. Valiev, Y. Estrin, Z. Horita, T.G. Langdon, M.J. Zehetbauer, Y.T. Zhu, Producing bulk ultrafine-grained materials by severe plastic deformation: Ten years later, JOM. 68 (2016) 1216-1226.

DOI: 10.1007/s11837-016-1820-6

Google Scholar

[2] M.P. Liu, X.F. Xie, Z.Y. Zhang, H. Wang, H.J. Roven, Deformation-induced solid-state amorphization in a nanostructured Al-Mg alloy processed by high pressure torsion, Mater. Sci. Forum. 817 (2015) 627-633.

DOI: 10.4028/www.scientific.net/msf.817.627

Google Scholar

[3] P.V. Liddicoat, X.Z. Liao, Y. Zhao, Nanostructural hierarchy increases the strength of aluminium alloys, Nature. Commun. 1 (2010) 63.

Google Scholar

[4] M.P. Liu, Z.J. Wu, R. Yang, J.T. Wei, Y.D. Yu, P.C. Skaret, H.J. Roven, DSC analyses of static and dynamic precipitation of an Al-Mg-S-Cu aluminum alloy, Prog. Nat. Sci.: Mater. Int. 25 (2015) 153-158.

DOI: 10.1016/j.pnsc.2015.02.004

Google Scholar

[5] C.H. Liu, X.L. Li, S.H. Wang, J.H. Chen, Q. Teng, J. Chen, Y. Gu, A tuning nano-precipitation approach for achieving enhanced strength and good ductility in Al alloys, Mater. Des. 54 (2014) 144-148.

DOI: 10.1016/j.matdes.2013.08.042

Google Scholar

[6] Z. Zhang, M.P. Liu, Y.D. Yu, P.C. Skaret, H.J. Roven, Microstructure characterization of an Al-Mg-Si aluminum alloy processed by equal channel angular pressing, Mater. Sci. Forum. 745-746 (2013) 303-308.

DOI: 10.4028/www.scientific.net/msf.745-746.303

Google Scholar

[7] L.P. Ding, Z.H. Jia, Z.Q. Zhang, R.E. Sanders, Q. Liu, G. Yang, The natural aging and precipitation hardening behaviour of Al-Mg-Si-Cu alloys with different Mg/Si ratios and Cu additions, Mater. Sci. Eng. A627 (2015)119-126.

DOI: 10.1016/j.msea.2014.12.086

Google Scholar

[8] H.J. Roven, M.P. Liu, J.C. Werenskiold, Dynamic precipitation during severe plastic deformation of an Al–Mg–Si aluminium alloy, Mater. Sci. Eng. A483-484 (2008) 54-58.

DOI: 10.1016/j.msea.2006.09.142

Google Scholar

[9] M.P. Liu, T.H. Jiang, X. F. Xie, Q. Liu, X. F. Li and H.J. Roven, Microstructure evolution and dislocation configurations in nanostructured Al-Mg alloys processed by high pressure torsion, Trans. Nonferrous Met. Soc. China, 24 (12) (2014).

DOI: 10.1016/s1003-6326(14)63542-1

Google Scholar

[10] M.P. Liu, S.C. Sun, H.J. Roven, Y.D. Yu, Z. Zhang, M.Y. Murashkin, R.Z. Valiev, Deformation defects and electron irradiation effect in nanostructured Al-Mg alloy processed by severe plastic deformation, Trans. Nonferrous Met. Soc. China, 2012, 22 (8), 1810-1816.

DOI: 10.1016/s1003-6326(11)61391-5

Google Scholar

[11] www. factsage. com.

Google Scholar

[12] T. Ungar, Characterization of nanocrystalline materials by X-ray line profile analysis, J. Mater. Sci. 42 (2007) 1584-1593.

Google Scholar

[13] M.P. Liu, T.H. Jiang, J. Wang, Q. Liu, Z.J. Wu, Y.D. Yu, P.C. Skaret and H.J. Roven, Aging behavior and mechanical properties in a 6013 aluminum alloy processed by severe plastic deformation, Trans. Nonferrous Met. Soc. China, 24 (12) (2014).

DOI: 10.1016/s1003-6326(14)63543-3

Google Scholar

[14] C.W. Zhao, Y.M. Xing, C.E. Zhou, P.C. Bai, Experimental examination of displacement and strain fields in an edge dislocation core, Acta Mater. 56 (2008) 2570-2575.

DOI: 10.1016/j.actamat.2008.01.045

Google Scholar

[15] M.P. Liu, H.J. Roven, M.Y. Murashkin, R.Z. Valiev, A. Kilmametov, Z. Zhang and Y.D. Yu, Structure and mechanical properties of nanostructured Al-Mg alloys processed by severe plastic deformation, J. Mater. Sci. 48 (2013) 4681-4688.

DOI: 10.1007/s10853-012-7133-4

Google Scholar

[16] X.H. An, S.D. Wu, Z.F. Zhang, Evolution of microstructural homogeneity in copper processed by high-pressure torsion, Scripta Mater. 63 (2010) 560-563.

DOI: 10.1016/j.scriptamat.2010.05.030

Google Scholar