Production of Single-Phase Hydroxyapatite Porous Bodies from Gypsum/Polystyrene

Article Preview

Abstract:

Porous bodies were produced using hydroxyapatite as a starting material, gypsum, high purity material, low cost and that can be molded into the desired shape. Also, beads of polystyrene polymer. The first step of this work was to produce porous gypsum blocks obtained by mixing gypsum, water and polystyrene. After drying, they were submerged in acetone solvent for solubilizing the polymer and pore formation. The porous hydroxyapatite was synthesized in a second stage, where the porous gypsum blocks were immersed in a solution of (NH4)2HPO4 0.5 mol L-1 to 100 ° C and pH 7.0-9.0 for 24 hours. From this method, it was possible to produce bodies single phase hydroxyapatite with a maximum porosity of 70 ± 3% and a compressive strength of 1.48 ± 0.17 MPa.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

187-192

Citation:

Online since:

November 2016

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2017 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] A.A. Barbosa, A.V. Ferraz, G.A. Santos:. Cerâmica Vol. 60 (356) (2014), p.501.

Google Scholar

[2] J.W.D. Callister: Ciência e Engenharia de Materiais: uma Introdução. LTC 7ª Ed. Rio de Janeiro, (2008).

Google Scholar

[3] Information on www. acepe. pt.

Google Scholar

[4] M. Amianti, V.R. Botaro: Revista Matéria Vol. 13 (4) (2008), p.664.

Google Scholar

[5] L.L. Hench: Journal of the American Ceramic Society Vol. 74 (7) (1991), p.1487.

Google Scholar

[6] J. Marchi et al.: Materials Research Bulletin Vol. 42 (2007), p.1040.

Google Scholar

[7] A.C.S. Dantas, et al.: Journal of the American Ceramic Society Vol. 91 (2008), p.1030.

Google Scholar

[8] A.C.S. Dantas, W. Acchar: Materials Science Forum Vols 798-799 (2014), 466.

Google Scholar

[9] L.L. Hench, J. Wilson: An Introduction to Bioceramics. (Florida vol. 1, 1993).

Google Scholar

[10] Associação Brasileira de Normas Técnicas. Método de ensaio. Rio de Janeiro: ABNT 1994. NBR 13207 / NBR 12128.

DOI: 10.12957/ric.2019.36907

Google Scholar

[11] A.A. Barbosa, et al.: Materials Research Vol. 17 (2014), p.39.

Google Scholar

[12] A.G.D. Azevedo, K. Strecker, H.F. Gorgulho: Cerâmica Vol. 61 (2015), p.52.

Google Scholar

[13] B. Cengiz et al.: Colloids and Surfaces A: Physicochem. Eng. Aspects Vol. 322 (2008), p.29.

Google Scholar

[14] P. Melnikov, et al.: Materials Chemistry and Physics Vol. 117 (2009), p.86.

Google Scholar

[15] D.S. Gouveia et al.: 17° Congresso Brasileiro de Ciência dos Materiais (CBECIMAT). Foz do Iguaçu 15-19 de Novembro 2006. Procceding.. Foz do Iguaçu 2006. (PR).

DOI: 10.21041/conpat2019/v2pat260

Google Scholar

[16] S.F. Hulbert, F.A. Young: J. Biomed. Material Research Vol. 4 (1970), p.433.

Google Scholar