Influence of Impurities on the Microstructure and Thermal Shock Resistance of YSZ Coatings

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The impact of impurities on the microstructure and thermal shock resistance of YSZ TBCs was investigated. ZrO2-7.5wt%Y2O3 (7.5YSZ) coatings of 5 spices of compositions (4 of them were doped with one type of impurity, namely, Al2O3, Fe2O3, SiO2 and TiO2, and the other was not doped) were manufactured by APS. Thermal shock tests of these TBCs were carried out at 1100 °C, and the samples were quenched in cold water in the temperature range from 20 to 25°C. The microstructure evolution and phase analysis were performed before and after the thermal shock tests by scanning electron microscope (SEM) and X-ray diffractometer (XRD). The results showed that the thermal shock lifetime of YSZ TBCs doped with impurities was obviously reduced compared to that of no-impurity TBCs. Additionally, the differences in the microstructure and phases of YSZ TBCs were ascertained and the elements distribution was tested by Energy Dispersive Spectrometer (EDS) and Energy Dispersive X-Ray Spectroscopy (EDX).

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1414-1423

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June 2017

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© 2017 Trans Tech Publications Ltd. All Rights Reserved

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