Characterization of Silica Extracted from Rice Husk Ash Wastes Doped by Tin Dioxide for Wave Guide Material

Abstract:

A series of experiments is made to produce silica, mixing with tin dioxide (SnO₂), and characterizing for application of waveguide device. Silica xerogels (SX) are prepared from raw materials derived from rice husks ash (RHA), which abundant in South East Sulawesi. The synthesis conditions have been optimized to obtain the ash of rice husks with the maximum silica content. SnO₂ are prepared from a commercial powder. The ceramic waveguide materials are produced by mixing SX and SnO₂ with various composition. The mixtures are molded to form the rectangular shape of 20 mm, 40 mm, and 5 mm in size. The samples will be sintered at different level of temperatures (from 300°C to 1200°C) by using microwave heating system as well as electric furnace. The microstructural of sintered samples were characterized on the basis of the experimental data obtained using densification measurement method (Archimedes method), crystallization (X-ray diffraction, XRD), microstructure (Scanning electron microscope, SEM). Optical and related properties such as the functional groups, structure, and absoption were characterized by using FTIR, Infrared and Raman Spectroscopy and absorption (UVVis). The permittivity and permeability will be calculated from S-parameters determined by using Vector Network Analyzer (VNA). Characterization results are presented in this paper and the others are will be published in another separated papers. Furthermore, the relationship between properties with SnO₂ content and sintering temperature is also studied.

• Periodical: Solid State Phenomena (Volume 266)
• Pages: 148-152
• DOI: https://doi.org/10.4028/www.scientific.net/SSP.266.148
• Online since: October 2017
• Authors: Inyoman Nyoman Sudiana*, Muhammad Zamrun Firihu, La Aba, La Ode Ngkoimani, Prima Endang Susilowati, Seitaro Mitsudo, Bambang Sunendar Purwasasmita, Komang Gde Suastika, Lina Lestari, Haji Aripin
• Keywords: Al₂O₃, Rice Husk Ash, Silica, Sintering Temperature, SnO₂, Waveguide Materials

References

[1] Dimitriev, Y., M. Bursukova, E. Kashchieva, V. Chernev and B. Samuneva. 1997, Journal of Sol- Gel Science and Technology, 8, p.937 – 940.

DOI: 10.1023/a:1018341131107

[2] Zaitoun, M. A., T. Kim, and C. T. Lin, 1998, J. Phys. Chem. B, 102.

[3] Pellegri, N., E. J. C. Dawnay, and E.M. Yeatman, 1998, Journal of Sol-Gel Science and Technology, 13, p.783.

DOI: 10.1023/a:1008630030373

[4] Xia, Z., G. Li, D. Chen, H. Xiao, 2009, Materials Letters, 63, p.2600 – 2602.

[5] Devi, S., and M. Srivastva, 2011. International Journal of Electronics Engineering, 3, p.51.

[6] Hunt, A. J., in: L. L Hench, J.K. West, 1992. Chemical processing of advance material, Willey, New York, p.341.

[7] Venkateswara Rao, A., P.B. Wagh, D. Haranath, P.P. Risbud, S.D. Kumbhare, 1999, Ceramics International, 25, p.505 – 509.

DOI: 10.1016/s0272-8842(97)00085-0

[8] Kalapathy, U, A. Proctor, J. Shultz, 2002, Bio Resource Technology, 85, p.285 – 289.

[9] Matori, K.A., M. M. Haslinawati, Z.A. Wahab, H.A.A. Sidek, T.K. Ban, W.A.W.A.K. Ghani, 2009, MASAUM Journal of Basic and Applied Sciences, 1, p.512 – 515.

[10] I. N. Sudiana, S. Mitsudo, M.Z. Firihu, L. Aba, L. O. Ngkoimani, M.W. Arsana, H. Aripin, AIP Conference Proceedings, 1801(1), 040003 (2017); DOI : 10. 1063/1. 4973092.

DOI: 10.1063/1.4973092

[11] I. N. Sudiana, S. Mitsudo, T. Nishiwaki, P. E. Susilowati, L. Lestari, M. Z. Firihu, H. Aripin, Journal of Physics: Conference Series, Vol. 739 No. 1, (2016) 012059.

DOI: 10.1088/1742-6596/739/1/012059

[12] Aripin, H., S. Mitsudo, I.N. Sudiana, S. Tani, K. Sako, Y. Fujii, T. Saito, T. Idehara, S. Sabchevski, 2011, Journal of Infrared, Millimeter and Terahertz Waves, 32, p.867 – 876.

DOI: 10.1007/s10762-011-9797-2

[13] H. Aripin, S. Mitsudo, E. S. Prima, I. N. Sudiana, S. Tani, K. Sako, Y. Fujii, T. Saito, T. Idehara, S. Sano, B. Sunendar, S. Sabchevski, J. of Infrared, Millimeter, and Terahertz waves, DOI 10. 1007/s10762-012-9925-7 (2012).

DOI: 10.1007/s10762-012-9925-7

[14] I. N. Sudiana, S. Mitsudo, M. Z. Firihu, H. Aripin, Materials Science Forum , Vo. 872, 2016, pp.114-117.

DOI: 10.4028/www.scientific.net/msf.872.114

[15] I. N. Sudiana, S. Mitsudo, M. Z. Firihu, Contemporary Engineering Sciences, Vol. 9, 2016, no. 12, 595-602.

[16] H. Aripin, S. Mitsudo, I.N. Sudiana, T. Saito, S. Sabchevski, , Transactions of the Indian Ceramic Society, DOI: 10. 1080/0371750X. 2014. 980850 (2015).

[17] I. N. Sudiana, S. Mitsudo, K. Sako, S. Inagaki, L. O. Ngkoimani, I. Usman, H. Aripin, AIP Conference Proceedings, 1719, 030014 (2016); doi: 10. 1063/1. 4943709.

DOI: 10.1063/1.4943709

[18] M. Zamrun F., I. N. Sudiana, S. Mitsudo, Contemporary Engineering Sciences, Vol. 9, 2016, 5, 237 – 247.

[19] I. N. Sudiana, Ryo Ito, S. Inagaki, K. Kuwayama, K. Sako, Seitaro Mitsudo, J. of Infrared, Millimeter, and Terahertz Waves, DOI 10. 1007/s10762-013-0011-6 (2013).

DOI: 10.1007/s10762-013-0011-6

[20] S. Mitsudo, S. Inagaki, I.N. Sudiana, K. Kuwayama, Advanced Materials Research, 789, pp.279-282 (2013).

DOI: 10.4028/www.scientific.net/amr.789.279

[21] S. Mitsudo, K. Sako, S. Tani, and I. N. Sudiana, High Power Pulsed Sub-Millimeter Wave Sintering Zirconia Ceramics, 36th International Conference on Infrared, Millimeter, and Terahertz Waves (IRMMW-THz) 2011, Oct 2-7, 2011, Hyatt Regency Houston, USA.

DOI: 10.1109/irmmw-thz.2011.6105135

[22] Y. L. Tian, D. L. Johnson, M. E. Brodwin, Vol. 1, Ceramic Powder Science II B. Edited by G. L. Messing, E. R. Fuller, and H. Hausner. American Ceramic Society Inc., Westerville, OH, (1988).

[23] C. Larsson, D. Sjoberg, and L. Elmkvist, 2010. Waveguide Measurements of The Permittivity and Permeability At Temperatures Up To 1000◦C . Lund University, Sweden.

DOI: 10.1109/tim.2011.2122150