The Influence of Temperature and Time in Electropolishing on Surface Roughness of Inner Surface of Stainless Steel 316l Cylinder for Pharmaceutical Industry Components

Article Preview

Abstract:

Surface cleanliness and smoothness are essential criteria for pharmaceutical components and they hold significant importance. Smooth surface minimizes bacterial accumulation and facilitates easier cleaning, promoting hygiene. In the pharmaceutical industry, equipment often employs electropolished tube pipes within machine components as conduits for processed medicinal solutions. Electropolishing is a widely-used electrochemical method involving a metal anode to achieve a smooth surface finish. This research is to investigate the impact of electropolishing temperature and time on the surface roughness of the inner surface of stainless steel 316L cylinders used in the pharmaceutical industry. Studying the influence of temperature and electropolishing time variations on the lowest surface roughness value inside a cylinder material, and identifying appropriate testing according to the ASME BPE surface roughness standard of less than 0.38 μm. Additionally, this study involves measuring the inner surface roughness, morphological characterization using metallurgical microscopy and SEM, as well as conducting potentiodynamic testing to assess the effectiveness of electropolishing. Based on the conducted experiments, it can be concluded that the lowest surface roughness value is found in samples subjected to a temperature variation of 60°C with a 7-minute EP duration, yielding an average surface roughness of 0.177 μm. Operational conditions that meet ASME BPE criteria (< Ra 3.8 μm) are achieved at electrolyte temperatures of 50°C and 60°C, with electropolishing process durations of 3-7 minutes. The lowest corrosion rate obtained was 0.00274 mpy with a surface roughness reduction of 70.50%, demonstrating the effectiveness of the electropolishing process.

You might also be interested in these eBooks

Info:

Periodical:

Solid State Phenomena (Volume 377)

Pages:

35-44

Citation:

Online since:

October 2025

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2025 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] L. B. Coelho et al., "Mechanical and corrosion characterization of industrially treated 316L stainless steel surfaces," Surf. Coatings Technol., vol. 382, p.125175, 2020.

DOI: 10.1016/j.surfcoat.2019.125175

Google Scholar

[2] Z. ur Rahman, K. M. Deen, L. Cano, and W. Haider, "The effects of parametric changes in electropolishing process on surface properties of 316L stainless steel," Appl. Surf. Sci., vol. 410, p.432–444, Jul. 2017.

DOI: 10.1016/j.apsusc.2017.03.081

Google Scholar

[3] K. Rokosz, T. Hryniewicz, S. Rzadkiewic, and S. Raaen, "Elektrolitičko poliranje nehrđajućeg čelika AISI 316L (EN 1.4404) uz visoku gustoću struje (HDEP)," Teh. Vjesn., vol. 22, no. 2, p.415–424, 2015.

DOI: 10.17559/TV-20140722110711

Google Scholar

[4] C. C. Lin, C. C. Hu, and T. C. Lee, "Electropolishing of 304 stainless steel: Interactive effects of glycerol content, bath temperature, and current density on surface roughness and morphology," Surf. Coatings Technol., vol. 204, no. 4, p.448–454, 2009.

DOI: 10.1016/j.surfcoat.2009.08.005

Google Scholar

[5] A. Raval, A. Choubey, C. Engineer, and D. Kothwala, "Surface conditioning of 316LVM slotted tube cardiovascular stents," J. Biomater. Appl., vol. 19, no. 3, p.197–213, 2005.

DOI: 10.1177/0885328205046564

Google Scholar

[6] J. R. (Joseph R. . Davis and ASM International. Handbook Committee., Stainless steels. ASM International, 1994.

Google Scholar

[7] W. D. Callister and D. G. Rethwisch, "Materials Science and Engineering: An Introduction", 10th ed., Hoboken, NJ: John Wiley & Sons, 2018..

Google Scholar

[8] S. A. Kukushkin, V. I. Blinov, and A. V. Osipov, "Microstructure and Corrosion Resistance of Ferritic and Martensitic Stainless Steels: A Review," Materials, 2019.

Google Scholar

[9] Outokumpu, "Handbook of Stainless steel," p.1–89, 2013.

Google Scholar

[10] E. Łyczkowska-Widłak, P. Lochyński, and G. Nawrat, "Electrochemical polishing of austenitic stainless steels," Materials (Basel)., vol. 13, no. 11, p.1–25, 2020.

DOI: 10.3390/ma13112557

Google Scholar

[11] A. Latifi, M. Imani, M. T. Khorasani, and M. D. Joupari, "Electrochemical and chemical methods for improving surface characteristics of 316L stainless steel for biomedical applications," Surf. Coatings Technol., vol. 221, p.1–12, 2013.

DOI: 10.1016/j.surfcoat.2013.01.020

Google Scholar

[12] S. N. Kane, A. Mishra, and A. K. Dutta, "Preface: International Conference on Recent Trends in Physics (ICRTP 2016)," J. Phys. Conf. Ser., vol. 755, no. 1, 2016.

DOI: 10.1088/1742-6596/755/1/011001

Google Scholar

[13] A. Q. A. Teo, L. Yan, A. Chaudhari, and G. K. O'neill, "Post-processing and surface characterization of additively manufactured stainless steel 316l lattice: implications for biomedical use," Materials (Basel)., vol. 14, no. 6, p.1–23, 2021.

DOI: 10.3390/ma14061376

Google Scholar

[14] E. Lyczkowska-Widlak, P. Lochynski, G. Nawrat, and E. Chlebus, "Comparison of electropolished 316L steel samples manufactured by SLM and traditional technology," Rapid Prototyp. J., vol. 25, no. 3, p.566–580, 2019.

DOI: 10.1108/RPJ-03-2018-0060

Google Scholar

[15] W. Han and F. Fang, "Eco-friendly NaCl-based electrolyte for electropolishing 316L stainless steel," J. Manuf. Process., vol. 58, no. September, p.1257–1269, 2020.

DOI: 10.1016/j.jmapro.2020.09.036

Google Scholar

[16] "Surface Texture ( Surface Roughness , Waviness , and Lay )," vol. 2009, 2009.

Google Scholar

[17] A. Bpe-, "Bioprocessing Equipment Bioprocessing Equipment," vol. 2016, 2016.

Google Scholar

[18] P.J. Núñez, E. García-plaza, M. Hernando, and R. Trujillo, "Characterization of Surface Finish of Electropolished Stainless steel AISI 316L with Varying Electrolyte Concentrations," Procedia Eng., vol. 63, p.771–778, 2013.

DOI: 10.1016/j.proeng.2013.08.255

Google Scholar

[19] P. Pendyala, M.S. Bobji, and G. Madras, "Evolution of surface roughness during electropolishing," Tribol. Lett., vol. 55, no. 1, p.93–101, 2014.

DOI: 10.1007/s11249-014-0336-x

Google Scholar

[20] H. Hocheng, P.S. Kao, and Y.F. Chen, "Electropolishing of 316L Stainless steel for Anticorrosion Passivation," vol. 10, no. August, p.414–418, 2001.

DOI: 10.1361/105994901770344827

Google Scholar

[21] S. J. Lee and J. J. Lai, "The effects of electropolishing (EP) process parameters on corrosion resistance of 316L stainless steel," J. Mater. Process. Technol., vol. 140, no. 1-3 SPEC., p.206–210, 2003.

DOI: 10.1016/S0924-0136(03)00785-4

Google Scholar

[22] P. Barnes et al., "Electropolishing valve metals with a sulfuric acid-methanol electrolyte at low temperature," Surf. Coatings Technol., vol. 347, no. 2017, p.150–156, 2018.

DOI: 10.1016/j.surfcoat.2018.04.082

Google Scholar

[23] B. Chatterjee, "Science and industry of electropolishing [Part 2)," Galvanotechnik, vol. 110, no. 2, p.255–262, 2019.

Google Scholar

[24] G. Yang, B. Wang, K. Tawfiq, H. Wei, S. Zhou, and G. Chen, "Electropolishing of surfaces: theory and applications," Surf. Eng., vol. 33, no. 2, p.149–166, 2017.

DOI: 10.1080/02670844.2016.1198452

Google Scholar

[25] E. S. Lee, "Machining characteristics of the electropolishing of stainless steel (STS316L)," Int. J. Adv. Manuf. Technol., vol. 16, no. 8, p.591–599, 2000.

DOI: 10.1007/s001700070049

Google Scholar

[26] S. Habibzadeh, L. Li, D. Shum-Tim, E. C. Davis, and S. Omanovic, "Electrochemical polishing as a 316L stainless steel surface treatment method: Towards the improvement of biocompatibility," Corros. Sci., vol. 87, p.89–100, 2014.

DOI: 10.1016/j.corsci.2014.06.010

Google Scholar

[27] S. Parker, Principles and Practice, vol. 32, no. 3. 2006.

DOI: 10.1177/0340035206070163

Google Scholar

[28] W. Han and F. Fang, "Fundamental aspects and recent developments in electropolishing," International Journal of Machine Tools and Manufacture, vol. 139. Elsevier Ltd, p.1–23, Apr. 2019.

DOI: 10.1016/j.ijmachtools.2019.01.001

Google Scholar

[29] A. M. Awad, E. A. Ghazy, S. A. Abo El-Enin, and M. G. Mahmoud, "Electropolishing of AISI-304 stainless steel for protection against SRB biofilm," Surf. Coatings Technol., vol. 206, no. 14, p.3165–3172, 2012.

DOI: 10.1016/j.surfcoat.2011.11.046

Google Scholar

[30] W.A.F. Base, "VoL. 2, No. 5, October, 1963," vol. 2, no. 5, p.1–2, 1963.

Google Scholar

[31] V. Sülar and A. Okur, "New application of a surface roughness tester on fabrics," AATCC Rev., vol. 7, no. 9, p.39–43, 2007.

Google Scholar

[32] C. A. I. Handbook, "ASM Metals Handbook, Volume 09 Metallography and Microstrustures Handbook," ASM Int., vol. 9, p.2733, 2004.

Google Scholar

[33] M. Ikhsan Almadani, R. Siswanto, and P. Studi Teknik Mesin, "Proses Manufaktur Mesin Poles Dan Ampelas Untuk Proses Metalografi," vol. 2, 2020.

DOI: 10.20527/jtam_rotary.v2i1.2001

Google Scholar

[34] M. Moshinsky, "No Title," Nucl. Phys., vol. 13, no. 1, p.104–116, 1959.

Google Scholar

[35] A. Cahyana and A. Marzuki, "Analisa SEM (Scanning Electron Microscope) pada Kaca TZN yang dikristalkan Sebagian," Pros. Math. Sci. Forum 2014, p.23–26, 2014.

Google Scholar

[36] Pierre R. Roberge, Handbook of Corrosion Engineering Library of Congress. 1999.

Google Scholar