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Online since: August 2004
Authors: Bernard Pieraggi, Didier Adé, Yannick Le Maoult
After compaction and thermomechanical processing, the alloy is recrystallised to generate a coarse
microstructure showing high grain aspect ratio to avoid as much as possible that the creep resistance
be impaired by grain boundary sliding or the formation of grain boundary creep pores.
Therefore, an estimate of εc can be obtained directly from only the measurement of height h of a larger number of trajectories.
Therefore, an estimate of εc can be obtained directly from only the measurement of height h of a larger number of trajectories.
Online since: September 2013
Authors: Shu Zhong Wang, Xiao Sun, Xiang Rong Luo, Xiao Juan Ren
Mainly because the sand ratio increases to a certain extent, proppant grain distribution is dense, the reunion phenomenon occurred in a fracturing fluid,and fracturing fluid viscosity makes the dense sand particles group act like a big particles, equivalent to greatly increase the particle diameter, causing particle settling velocity increase.This phenomenon is also referred to as "particle reunion" effect.
3.4 correlations for critical sedimentation velocity and particle settling velocity
Through the analysis of the above experimental results, considering the influences of sand ratio, temperature and foam quality on proppant settling velocity and critical settling velocity of fracturing fluid, the type(1) and (2) are fitting results to show correlations form calculated the particle settling velocity ut and critical settling velocity Vcr of fracturing fluid, the average error are 12.32% and 13.5% respectively:
The proppant grain density is about 1700 kg·m-3. the type scope of application is: 0≤CS≤10%, 10%≤Г≤85%, 40℃≤T≤80℃, P=10MPa
Conclusion 1)The proppant transport experimental results show that with increase of the temperature, the proppant grain in GRF-CO2 foam fracturing fluid sedimentation rate increases,at the same time, the fracturing fluid critical settling velocity increase, showing the proppant transport performance degradation. 2)Under the condition of foaming, with increase of the foam quality, proppant particle settling velocity reduces, fracturing fluid critical settling velocity reduces, proppant transport performance increases;The change law under not foaming condition is just the opposite.
:“Thermophysical Properties of Fluid Systems” in MIST Chemistry WebBook, NIST Standard Reference DataBase Number 69, Eds.
The proppant grain density is about 1700 kg·m-3. the type scope of application is: 0≤CS≤10%, 10%≤Г≤85%, 40℃≤T≤80℃, P=10MPa
Conclusion 1)The proppant transport experimental results show that with increase of the temperature, the proppant grain in GRF-CO2 foam fracturing fluid sedimentation rate increases,at the same time, the fracturing fluid critical settling velocity increase, showing the proppant transport performance degradation. 2)Under the condition of foaming, with increase of the foam quality, proppant particle settling velocity reduces, fracturing fluid critical settling velocity reduces, proppant transport performance increases;The change law under not foaming condition is just the opposite.
:“Thermophysical Properties of Fluid Systems” in MIST Chemistry WebBook, NIST Standard Reference DataBase Number 69, Eds.
Online since: April 2020
Authors: Radka Pernicová, Tomas Kolomaznik
Over the past decades, a large number of plasticizing additives have been marketed, which have been fundamentally different in chemical composition and have different plasticizing effects.
It can be new (only crushed to the desired grain size) or recycled (reuse of originally new SiC or use of SiC from waste processes such as filter dust or debris from sample crushing) [10, 11].
It is a suspension made from crystalline grains containing nanoparticles, the so-called “seeding technology”.
Ribakov at al.: Using Granite Siftings for Producing Vibro-Pressed Fine-Grained Concrete.
It can be new (only crushed to the desired grain size) or recycled (reuse of originally new SiC or use of SiC from waste processes such as filter dust or debris from sample crushing) [10, 11].
It is a suspension made from crystalline grains containing nanoparticles, the so-called “seeding technology”.
Ribakov at al.: Using Granite Siftings for Producing Vibro-Pressed Fine-Grained Concrete.
Online since: May 2020
Authors: Chong Sheng Long, Tian Guo Wei, Jun Song Zhang, Zhong Bo Yang, Jing Jing Liao
Matsuda et al. [6] have shown that grain boundary diffusion of oxygen dominates the initial oxide growth process for Zirconium alloys.
Many large grains that is larger than 10 um in diameter and obvious cracks on surface can be seen by Laser Scanning Confocal Microscope (LSCM).
The transition area is able to tolerate a large number of sub-stoichiometry oxide phase and disorders through a second-order mechanism.
Furthermore, the crystal grains gradually grow larger because of the high temperature.
Many large grains that is larger than 10 um in diameter and obvious cracks on surface can be seen by Laser Scanning Confocal Microscope (LSCM).
The transition area is able to tolerate a large number of sub-stoichiometry oxide phase and disorders through a second-order mechanism.
Furthermore, the crystal grains gradually grow larger because of the high temperature.
Online since: May 2021
Authors: Tjipto Sujitno, Suprapto Suprapto, Agung Setyo Darmawan, Dicky Efendi Surya Putra, Ridhwan Rafi Pangestu
The results of plasma nitrocarburizing at 570 °C showed the highest surface hardness, highest wear resistance and lowest coefficient of friction due to the number of phases ε.
The α-Ti phase had equiaxed grain.
The grain structure (spectrum 1) on the surface contains 27.39% titanium atoms, 45.42% nitrogen atoms and 27.19% carbon atoms.
The grain structure at cp titanium surface has a higher nitrogen and carbon content than dark areas and light areas.
The α-Ti phase had equiaxed grain.
The grain structure (spectrum 1) on the surface contains 27.39% titanium atoms, 45.42% nitrogen atoms and 27.19% carbon atoms.
The grain structure at cp titanium surface has a higher nitrogen and carbon content than dark areas and light areas.
Online since: April 2011
Authors: Hendi Saryanto, Pudji Untoro, Darwin Sebayang, M.A. Othman, T. Sujitno, Deni S. Khaerudini
Technical requirements to be used as interconnect in SOFC should fulfil a number of specific requirements, i.e. a high oxidation resistance, a high electrical conductivity of the surface oxide scales, gas tightness, and a coefficient of thermal expansion matched to the electrolyte and the electrodes [1,2].
The surfaces of Fe80Cr20-53.33 and 38.51 nm were covered with compact oxide scale consisting of fine grain scales (Fig. 4a and b).
For the as commercial ferritic steels show coarser grain scales with the big nodules and spallation across the surface of specimen (Fig. 4d and f), but for the implanted specimen, it show better in finer nodule.
The scale on the surface specimen Fe80Cr20-53.33 nm indicated fine grained and discontinuous (Fig.5a).
The surfaces of Fe80Cr20-53.33 and 38.51 nm were covered with compact oxide scale consisting of fine grain scales (Fig. 4a and b).
For the as commercial ferritic steels show coarser grain scales with the big nodules and spallation across the surface of specimen (Fig. 4d and f), but for the implanted specimen, it show better in finer nodule.
The scale on the surface specimen Fe80Cr20-53.33 nm indicated fine grained and discontinuous (Fig.5a).
Online since: October 2013
Authors: Wei Wu, Ran Liu, Bing Bing Liu, Xu Zou, Quan Jun Li, Ze Peng Li
The transparent powder grains were found to become translucent at the phase transition as had previously been observed.[9,10] It is clear that pressure induced changes to the diffraction pattern of walnut GeO2 were observed above 8.99 GPa.
It is worthymetioned that the high pressure behavior of GeO2 bulk materials remains under controversy. [9-11] Itie et al, [11] reported a transition occurred above 6 GPa at which the germanium coordination number increases from four to six by EXAFS.
As the nano-crystalline b-GeO2 sample are of an average grain size of 20nm.
As a result, the high pressure phase transition of b-GeO2 to monoclinic phase may occur on the grain boundary of these nano particles. [18b] but further studies are still needed.
It is worthymetioned that the high pressure behavior of GeO2 bulk materials remains under controversy. [9-11] Itie et al, [11] reported a transition occurred above 6 GPa at which the germanium coordination number increases from four to six by EXAFS.
As the nano-crystalline b-GeO2 sample are of an average grain size of 20nm.
As a result, the high pressure phase transition of b-GeO2 to monoclinic phase may occur on the grain boundary of these nano particles. [18b] but further studies are still needed.
Online since: October 2014
Authors: Mei Lin, Xiao Wu, Bo Lei Chen, Ji Kang Yuan
While for pH = 9, the platelet-like grains accumulate with each other to form the symmetrical hexagram-like LFP, with the size of about 25 µm (Fig. 1c, 1d).
The platelet-like structure transforms to porous spindle one with a large number of holes on the surface of LFP sample, as shown in Fig. 2a and Fig. 2b.
When the reaction condition is pH = 9 for 24 h (Fig. 2c, 2d), the LFP sample shows the corn cob-like microstructure with the average length of 3 µm for each grain.
The SEM studies indicate that pH condition and reaction time remarkably influence both the morphologies and grain size of LFP samples.
The platelet-like structure transforms to porous spindle one with a large number of holes on the surface of LFP sample, as shown in Fig. 2a and Fig. 2b.
When the reaction condition is pH = 9 for 24 h (Fig. 2c, 2d), the LFP sample shows the corn cob-like microstructure with the average length of 3 µm for each grain.
The SEM studies indicate that pH condition and reaction time remarkably influence both the morphologies and grain size of LFP samples.
Online since: May 2023
Authors: Xi Wu Li, Bai Qing Xiong, Guan Jun Gao, Zheng An Wang, Kai Wen, Li Fang Chen
.%)
Alloy number
Zn
Mg
Cu
Zr
Fe
Si
LFS alloy
7.46
1.69
1.64
0.11
<0.01
<0.01
MFS alloy
7.46
1.69
1.67
0.11
0.03
0.02
HFS alloy
7.46
1.69
1.67
0.11
0.08
0.06
Results and Discussion
Microstructure analysis for as-cast and as-homogenized alloys
Fig. 1(a-c) shows the OM microstructure of the three alloys.
It can be easily observed from the OM images that apparent eutectic structure with net-like characteristics exists on grain boundary while the dendritic structure of them is similar.
From Fig. 4(a-c) we can see that abundant second phases with small size and relatively coarsen phases exist on grain boundary.
Some of them distribute in the matrix while the others lie on grain boundary.
It can be easily observed from the OM images that apparent eutectic structure with net-like characteristics exists on grain boundary while the dendritic structure of them is similar.
From Fig. 4(a-c) we can see that abundant second phases with small size and relatively coarsen phases exist on grain boundary.
Some of them distribute in the matrix while the others lie on grain boundary.
Online since: February 2016
Authors: Beata Leszczyńska-Madej, Anna Tylek, Albert Zygiert
The microstructure of obtained as-sinters (Fig.6-7) consist of mostly regular aluminum grains with dissolved copper in it and precipitations corresponding to the Al-Cu phase diagram.
On grain boundaries the pores, formed by incomplete consolidation of powders during compaction and sintering, are visible.
During slow cooling of aluminum alloy contains 4% of copper from α single-phase solution area to room temperature the large precipitations of ө phase forms on the grain boundaries of α solution.
The financial support of the State Committee for Scientific Research of Poland under the grant number 11.11.180.653 is kindly acknowledged.
On grain boundaries the pores, formed by incomplete consolidation of powders during compaction and sintering, are visible.
During slow cooling of aluminum alloy contains 4% of copper from α single-phase solution area to room temperature the large precipitations of ө phase forms on the grain boundaries of α solution.
The financial support of the State Committee for Scientific Research of Poland under the grant number 11.11.180.653 is kindly acknowledged.