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Online since: January 2012
Authors: Nazanin Farhadyar, Mirabdullah Seyed Sadjadi
Synthesis and Characterization of ZnO-SiO2/Epoxy Nanocomposite Coating by Sol-gel Process
Nazanin Farhadyar1,a, Mirabdullah Seyed Sadjadi2,b
1Department Chemistry, Islamic Azad University, Varamin-pishva Branch, Varamin, 33817-74895, Iran
2Department Chemistry, Science and Research Branch, Islamic Azad University, Tehran,14778-93855, Iran
anfarhadyar@gmail.com (corresponding author), bm.s.sadjad@gmail.com
[Don’t type anything in this line, it’ll show the date of receipt and acceptance]
Keywords: Hybrid material; Sol-gel; Nanocomposite; ZnO/Epoxy
Abstract.
Attenuated total reflectance infrared spectroscopic (ATR-IR) technique was used to characterize the structure of the hybrid films.
The chemical structure of obtained network affects morphology of the coating.
The hybrid systems have a unit form structure and the inorganic phases were in the nanosize scale, Introduction Nanocomposite coating films on glass substrates are important for applications such as window glass, mirrors, and windshields of automobiles, and so on [1] and [2].
Another factor affecting the hydrophilic property is the chemical structure of the surfaces.
Attenuated total reflectance infrared spectroscopic (ATR-IR) technique was used to characterize the structure of the hybrid films.
The chemical structure of obtained network affects morphology of the coating.
The hybrid systems have a unit form structure and the inorganic phases were in the nanosize scale, Introduction Nanocomposite coating films on glass substrates are important for applications such as window glass, mirrors, and windshields of automobiles, and so on [1] and [2].
Another factor affecting the hydrophilic property is the chemical structure of the surfaces.
Online since: April 2016
Authors: Liang Chao Li, Juan Bi Li, Di Qiong Hu, Yan Ding, Yu Huan Wang
The crystal structure and composition, electrical conductivity, optical rotation, dielectric loss and magnetic loss of the as-prepared samples were researched.
It was also discovered that chiral material with good conductivity due to its unique structure and properties has shown a higher microwave absorption performance[4].
Results and discussion Structure andcomposition.
The FT-IR spectra of CFO confirms that the absorption peaksof570 cm-1and 416 cm-1belong to the spinel structure.
Yuan, N.Kuramoto: Chemistry Letters. 31 (2002) 544
It was also discovered that chiral material with good conductivity due to its unique structure and properties has shown a higher microwave absorption performance[4].
Results and discussion Structure andcomposition.
The FT-IR spectra of CFO confirms that the absorption peaksof570 cm-1and 416 cm-1belong to the spinel structure.
Yuan, N.Kuramoto: Chemistry Letters. 31 (2002) 544
Online since: August 2015
Authors: Mahidin Mahidin, Zuhra Zuhra, Fikri Hasfita, Husni Husin, Yunardi Yunardi
The results showed that the XRD pattern of the La-C-co-doped NaTaO3 was found to be crystalline phase with orthorhombic structure.
Thus, anion and cation doping can adjust the band structure of semiconductors, and it can also have an impact on the particle size and surface structure of materials [13], which usually results in a better photocatalytic activity [14].
Petrik, Preparation of visible-light responsive N-F-co-doped TiO2 photocatalyst by a sol–gel-solvothermal method, Journal of Photochemistry and Photobiology A: Chemistry 184 (2006) 282-288
Wu, Synthesis of nanosized NaTaO3 in low temperature and its photocatalytic performance, Journal of Solid State Chemistry, 177 (2004) 3868-3872
Liang, Photocatalytic degradation of organic pollutants with Ag decorated free-standing TiO2 nanotube arrays and interface electrochemical response, Journal of Materials Chemistry, 21 (2011) 475-480
Thus, anion and cation doping can adjust the band structure of semiconductors, and it can also have an impact on the particle size and surface structure of materials [13], which usually results in a better photocatalytic activity [14].
Petrik, Preparation of visible-light responsive N-F-co-doped TiO2 photocatalyst by a sol–gel-solvothermal method, Journal of Photochemistry and Photobiology A: Chemistry 184 (2006) 282-288
Wu, Synthesis of nanosized NaTaO3 in low temperature and its photocatalytic performance, Journal of Solid State Chemistry, 177 (2004) 3868-3872
Liang, Photocatalytic degradation of organic pollutants with Ag decorated free-standing TiO2 nanotube arrays and interface electrochemical response, Journal of Materials Chemistry, 21 (2011) 475-480
Online since: October 2010
Authors: Cong Jie Gao, Li Wang, Duo Wang, Gui Ru Zhu
Synthesis of Highly Mono-dispersed Mesoporous Silica Spheres
Guiru Zhu1, a, Li Wang1, b, Duo Wang1, c, Congjie Gao1, d
1Key Laboratory of Marine Chemistry Theory and Technology, Ministry of Education, College of Chemistry and Chemical Engineering, Ocean University of China, Qingdao 266100, China
azhugr@ouc.edu.cn, b wangli19841123@163.com, cwangduo@ouc.edu.cn, d gaocjie@mail.hz.zj.cn,
Keywords: Mesoporous silica; Sphere; Mono-dispersed
Abstract.
The results showed that the synthesized mono-dispersed spherical silica particles have ordered hexagonal mesoporous structure, high specific surface area and uniform pore size distribution.
The XRD patterns of the materials synthesized with similar methanol ratio and temperature are almost same, suggesting that the concentration of C16TAC (Fig. 5-A) and TEOS (Fig. 5-B) have little influence on the orderity of the mesoporous structure.
It indicated that the influence of the amount of methanol on the mesoporous structure is weak.
It is assumed that parallel alignment of surfactants at the surface of the particles leads to a radially aligned mesoporous structure [17].
The results showed that the synthesized mono-dispersed spherical silica particles have ordered hexagonal mesoporous structure, high specific surface area and uniform pore size distribution.
The XRD patterns of the materials synthesized with similar methanol ratio and temperature are almost same, suggesting that the concentration of C16TAC (Fig. 5-A) and TEOS (Fig. 5-B) have little influence on the orderity of the mesoporous structure.
It indicated that the influence of the amount of methanol on the mesoporous structure is weak.
It is assumed that parallel alignment of surfactants at the surface of the particles leads to a radially aligned mesoporous structure [17].
Online since: December 2012
Authors: Gui Yang Liu, Bao Sen Wang, Ying He, Jun Ming Guo
The phase structures are characterized by X-ray diffraction (XRD).
The possible reasons responsible for the quick fading of capacity are generally believed to the Jahn-Teller distortion of the cubic spinel structure of LiMn2O4.
With increasing Mn3+ in the structure, Mn3+ was gradually dissolved to electrolyte via disproportionation reaction, and the organic solvent was decomposed at higher potentials [4].
It is well known that LiMn2O4 takes the face-centered cubic framework of spinel structure with Fd3m space group, in which the Li+ ions occupy the tetrahedral 8a sites, while the Mn3+, Mn4+ (and the doping Ni3+) ions reside at the octahedral 16d sites, and the O2− ions are located at the 32e sites [16].
Acknowledgements The present work was supported by the National Natural Science Foundation of China (No.51062018) and by the Key Subject of Materials Physics and Chemistry of Honghe University.
The possible reasons responsible for the quick fading of capacity are generally believed to the Jahn-Teller distortion of the cubic spinel structure of LiMn2O4.
With increasing Mn3+ in the structure, Mn3+ was gradually dissolved to electrolyte via disproportionation reaction, and the organic solvent was decomposed at higher potentials [4].
It is well known that LiMn2O4 takes the face-centered cubic framework of spinel structure with Fd3m space group, in which the Li+ ions occupy the tetrahedral 8a sites, while the Mn3+, Mn4+ (and the doping Ni3+) ions reside at the octahedral 16d sites, and the O2− ions are located at the 32e sites [16].
Acknowledgements The present work was supported by the National Natural Science Foundation of China (No.51062018) and by the Key Subject of Materials Physics and Chemistry of Honghe University.
Online since: September 2020
Authors: Nadiah Bte Ameram, Arlina Ali, Nik Alnur Auli
The additions of TiO2 shift the structure of YBCO system from rhombic to tetragonal structure.
This resulted in a large percentage of tetragonal structure in the YBCO system.
From the XRD the dominant phase was YBCO with orthorhombic crystal structure.
Materials chemistry and Physics, 61(3), 251-259
Journal of Physics and Chemistry of solids, 64(2), 273-280.
This resulted in a large percentage of tetragonal structure in the YBCO system.
From the XRD the dominant phase was YBCO with orthorhombic crystal structure.
Materials chemistry and Physics, 61(3), 251-259
Journal of Physics and Chemistry of solids, 64(2), 273-280.
Online since: December 2014
Authors: Francisco Pinto Filho, Crislene Rodrigues da Silva Morais, Karla Valéria Miranda de Campos, José Jefferson da Silva Nascimento, Josué da Silva Burit
Characterized the crystal structures of these materials by diffraction of X-ray and mechanical behavior using tensile test.
The technique of X-ray diffraction was used as a tool to verify the phases that are present in the alloy steel submitted appropriate crystal structures.
Although aimed at the control of the austenitic phase in the steel structure, the use of this element is inappropriate for steels with orthopedic purposes.
Ultimately, stainless steel studied in this work showed off the chemistry which was established by the standard reference composition.
The diffractogram shown in Figure 1 shows the crystal structure of the stainless steel alloy studied in this work.
The technique of X-ray diffraction was used as a tool to verify the phases that are present in the alloy steel submitted appropriate crystal structures.
Although aimed at the control of the austenitic phase in the steel structure, the use of this element is inappropriate for steels with orthopedic purposes.
Ultimately, stainless steel studied in this work showed off the chemistry which was established by the standard reference composition.
The diffractogram shown in Figure 1 shows the crystal structure of the stainless steel alloy studied in this work.
Online since: March 2013
Authors: Jia Sun, Xin Zhong Liu, Lei Peng
The situ method (also known as activated swelling method) can prepares monodisperse superparamagnetic microspheres with a mixed structure.
Song: Chemistry and Industry of Forest Products, Vol. 19 (1999) No.3, p.79
Chu: Chemistry and Industry of Forest Products, Vol.29 (2009) No.3, p25
Bisson: Analytical Chemistry, Vol. 51 (1979) No.7, p.844
Wang: Environmental Chemistry, Vol. 21 (2002) No.5, p.430
Song: Chemistry and Industry of Forest Products, Vol. 19 (1999) No.3, p.79
Chu: Chemistry and Industry of Forest Products, Vol.29 (2009) No.3, p25
Bisson: Analytical Chemistry, Vol. 51 (1979) No.7, p.844
Wang: Environmental Chemistry, Vol. 21 (2002) No.5, p.430
Online since: August 2018
Authors: Yunas Jumril, Sulaiman Noor Humam, Mariyam Jameelah Ghazali
Analysis results through XRD showed that an orthorhombic structure of calcium ferrite NPs was observed.
The structure, the physical and magnetic properties of the synthesized nanoparticles have been analyzed.
The XRD result confirms the orthorhombic structure with crystal size of approximately 16.8 nm.
Journal of Materials Chemistry 17 (2007) 4876- 4884
Chemistry Central Journal, 5, pp. 19
The structure, the physical and magnetic properties of the synthesized nanoparticles have been analyzed.
The XRD result confirms the orthorhombic structure with crystal size of approximately 16.8 nm.
Journal of Materials Chemistry 17 (2007) 4876- 4884
Chemistry Central Journal, 5, pp. 19
Online since: April 2013
Authors: Cheng Tung Chong, Simone Hochgreb
The global flame structure of flame and flow field were investigated at the fixed power output of 6 kW.
Spray flame involves the complex interaction of air, fuel and chemistry.
Understanding spray flame requires detailed investigation of the spray droplets, flow field, chemistry reaction, flame structure and the interactions between these factors.
This paper focuses on the global flame structure within the combustor.
Flame imaging technique is employed to study the flame structure.
Spray flame involves the complex interaction of air, fuel and chemistry.
Understanding spray flame requires detailed investigation of the spray droplets, flow field, chemistry reaction, flame structure and the interactions between these factors.
This paper focuses on the global flame structure within the combustor.
Flame imaging technique is employed to study the flame structure.