Catalytic Synthesis of Benzyl Acetate by Diatomite Supported Waugh-Type (NH4)6[MnMo9O32] •8H2O

Shu Heng Liu

doi:10.4028/www.scientific.net/AMM.483.38

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HomeApplied Mechanics and MaterialsApplied Mechanics and Materials Vol. 483Catalytic Synthesis of Benzyl Acetate by Diatomite...

Catalytic Synthesis of Benzyl Acetate by Diatomite Supported Waugh-Type (NH₄)₆[MnMo₉O₃₂] •8H₂O

Abstract:

Take Waugh-Type (NH₄)₆[MnMo₉O₃₂] •8H₂O absorbed on diatomite and prepared supported solid catalyst. The properties of the catalyst were studied through the synthesis of benzyl acetate. The appropriate reaction conditions were obtained by orthogonal test: mole ratio of acetic acid to benzyl alcohol was 2.5:1.0, the catalyst dosage was 1.6g, the water carrying agent toluene dosage was 2.5ml, reaction time was 150min, esterification yield was 87.4%. The catalyst are high catalytic activity and non- polluting, and could be reused.

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Periodical:

Applied Mechanics and Materials (Volume 483)

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38-41

DOI:

https://doi.org/10.4028/www.scientific.net/AMM.483.38

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Online since:

December 2013

Authors:

Shu Heng Liu

Keywords:

Benzyl Acetate, Diatomite Supported, Waugh-Type

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