Synthetic Study towards Salvianolic Acid A: Synthesis of the Intermediate of (3, 4-Bis((Tert-Butyldimethylsilyl)Oxy)-Benzylidene)Triphenylphosphorane

Li Ping Wang; Dong Wang Liu; Shuang Lin Qin; Gao Peng Wang; Xiao Ji Wang; Shuang Ping Huang

doi:10.4028/www.scientific.net/AMR.1033-1034.573

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 1033-1034Synthetic Study towards Salvianolic Acid A:...

Synthetic Study towards Salvianolic Acid A: Synthesis of the Intermediate of (3, 4-Bis((Tert-Butyldimethylsilyl)Oxy)-Benzylidene)Triphenylphosphorane

Abstract:

Synthesis of (3, 4-bis ((tert-butyldimethylsilyl) oxy)-benzylidene) triphenyl- phosphorane, an important intermediate of salvianolic acid A (1), was reported, which synthetic route including protection, bromation and Wittig salt formation.

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Periodical:

Advanced Materials Research (Volumes 1033-1034)

Pages:

573-575

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.1033-1034.573

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Online since:

October 2014

Authors:

Li Ping Wang*, Dong Wang Liu, Shuang Lin Qin, Gao Peng Wang, Xiao Ji Wang, Shuang Ping Huang

Keywords:

(3, 4-Bis((Tert-Butyldimethylsilyl)Oxy)-Benzylidene)Triphenylphosphorane, Salvianolic Acid, Synthesis

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References

[1] Jae-Hak Moon, Hyoung Jae Lee, Jeong-Yong Cho. Fitoterapia. 2012, 83, 1196-1204.

Google Scholar

[2] Philippe Cotelle, Vincent Dalla. Tetrahedron. 1998, 39, 8285-8286.

Google Scholar

[3] Philippe Cotelle, Vincent Dalla. Tetrahedron. 1999, 55, 6923-6930.

Google Scholar

[4] Zheng-Fu Zhang, Zong-Gen Peng, Lei Gao, Biao Dong, Jian-Rui Li, Zhuo-Yong Li, Hong-Shan Chen. J. Asian Nat. Prod. Res., 2008, 10, 391-396.

Google Scholar

[5] Masanobu Uchiyama, Hiroki Ozawa, Kazuya Takuma, Yotaro Matsumoto, Mitsuhiro Yonehara, Kou Hiroya, Takao Sakamoto. Org. Lett, 2006, 8, 5517-5520.

DOI: 10.1021/ol062190+

Google Scholar

[6] Minoru Ishikawa, Kazunori Motoshima, Tomomi Noguchi-Yachide, Kazuyuki Sugita, Yuichi Hashimoto. Bioorg. Med. Chem. 2009, 17, 5001–5014.

Google Scholar