Carbon Fiber Reinforced SiC Matrix Composites Fabricated by Preceramic Impregnation and Pyrolysis Process Combining SiC Nano Powder Infiltration

Jing Jing Wang; Wen Song Lin; Li Hui Duan; Xue Zeng Yan

doi:10.4028/www.scientific.net/AMR.1052.34

Paper Titles

High Speed Extrusion Rheological Behavior Analysis of Marine ABS/PC Alloy
p.14

First-Principle Studies on the Stability of AlN(0001)/NbB₂(0001) Interface
p.18

Mechanical Properties and Toughening Mechanisms of Multi-Walled Carbon Nanotube Reinforced Yttria-Stabilized Zirconia Composite
p.24

Energetic Studies on the B Effect on the Oxidation of γ-TiAl Alloys
p.28

Carbon Fiber Reinforced SiC Matrix Composites Fabricated by Preceramic Impregnation and Pyrolysis Process Combining SiC Nano Powder Infiltration
p.34

Fabrication of TiB₂/TiC Duplex Particles Reinforced Carbon Steel Matrix Surface Composite
p.40

Static Recrystallization and Texture Evolution of 316L Stainless Steel Fibers
p.45

Research in an Original Si-Mn-Mo-Nb 800MPa Dual Phase Steel with Low Carbon
p.51

Effect of Copper Content on Mechanical Properties of Short Carbon Fiber Reinforced ZrC Mateix Composites
p.55

HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 1052Carbon Fiber Reinforced SiC Matrix Composites...

Carbon Fiber Reinforced SiC Matrix Composites Fabricated by Preceramic Impregnation and Pyrolysis Process Combining SiC Nano Powder Infiltration

Abstract:

SiC nanopowder, polycarbosilane and divinylbenzene mixed slurries were prepared for viscosity measurement, which were used as matrix source of ceramic matrix composites. Results showed that apparent viscosity of the slurries increased with the increase of the content of SiC particles. The slurries with 50 nm SiC particles showed a low viscosity as compared with those slurries with 20 nm or 120 nm SiC particles at the same content of SiC. In particular, when the viscosity of slurry was higher than 30 mPa•s, the slurry could not be used in the test. Three-dimensional carbon fiber (3D-C_f) preforms were infiltrated with the aforementioned slurries. Addition of the nanoSiC powder as the inert filler in the slurries led to reduce the porosity and the infiltration–curing–pyrolysis cycles to manufacture 3D-C_f/SiC composites by the subsequent polymer impregnation and pyrolysis (PIP) process. Characterizations of the composites showed that the maximum flexural strength of specimen in the composites was 326 MPa and its fracture toughness was 10.5 MPa•m^1/2.

You might also be interested in these eBooks

Innovative Materials: Engineering and Applications

View Preview

Info:

Periodical:

Advanced Materials Research (Volume 1052)

Pages:

34-39

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.1052.34

Citation:

Cite this paper

Online since:

October 2014

Authors:

Jing Jing Wang, Wen Song Lin*, Li Hui Duan, Xue Zeng Yan

Keywords:

Inert Filler, Polycarbosilane, Polymer Impregnation, Polymer Pyrolysis, Silicon Carbide (SiC), Viscosity

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

* - Corresponding Author

References

[1] X.G. Zhou, Y. You, C.R. Zhang, B.Y. Huang, X.Y. Liu, Effect of carbon fiber pre-heat treatment on the microstructure and properties of Cf/SiC composites, Mater. Sci. Eng. A 433(2006)104–107.

Google Scholar

[2] R. Dong, Y. Hirata, H. Sueyoshi, M. Higo, Y. Uemura, Polymer impregnation and pyrolysis (PIP) method for the preparation of laminated woven fabric/mullite matrix composites with pseudoductility, J. Eur. Ceram. Soc. 24(2004)53-64.

DOI: 10.1016/s0955-2219(03)00127-4

Google Scholar

[3] R.M. Rocha, C.A.A. Cairo, M.L.A. Graca, Formation of carbon fiber reinforced ceramic matrix composites with polysiloxane/silicon derived matrix, Mater. Sci. Eng. A: Struct. Mater. Prop. Microstruct. Process. 437(2) (2006)268-273.

DOI: 10.1016/j.msea.2006.08.102

Google Scholar

[4] H.F. Hu, Q.K. Wang, Z.H. Chen, C.R. Zhang, Y.D. Zhang, J. Wang, Microstructure observation and analysis of 3D carbon fiber reinforced SiC-based composites fabricated through filler enhanced polymer infiltration and pyrolysis, Ceram. Intern. 38 (2012).

DOI: 10.1016/j.ceramint.2011.07.039

Google Scholar

[5] D.H. Ding, W.C. Zhou, F. Luo, M.L. Chen, D.M. Zhu, Mechanical properties and oxidation resistance of SiCf/CVI-SiC composites with PIP-SiC interphase, Ceram. Intern. 38(2012)3929-3934.

DOI: 10.1016/j.ceramint.2012.01.045

Google Scholar

[6] R. Naslain, F. Langlais, G. Vignoles, R. Pailler, The CVI-process: state of the art and perspective, Ceram. Eng. Sci. Proc. 27(2006)373-86.

DOI: 10.1002/9780470291313.ch37

Google Scholar

[7] X. Yang, Z. Su, Q.Z. Huang, X. Fang, L.Y. Chai, Microstructure and Mechanical Properties of C/C–ZrC–SiC Composites Fabricated by Reactive Melt Infiltration with Zr, Si Mixed Powders, J. Mater. Sci. Tech. 29(2013)702-710.

DOI: 10.1016/j.jmst.2013.05.005

Google Scholar

[8] Y.G. Wang, X.J. Zhu, L.T. Zhang, L.F. Cheng, C/C–SiC–ZrC composites fabricated by reactive melt infiltration with Si0. 87Zr0. 13 alloy, Ceram. Intern. 38(2012)4337-4343.

DOI: 10.1016/j.ceramint.2012.02.016

Google Scholar

[9] X. Yang, H.F. Hu, Y.D. Zhang, Z.H. Chen, Thermal shock properties of 3D-C/SiC composites prepared via polymer infiltration pyrolysis (PIP), Ceram. Intern. A40(2014)9087-9094.

DOI: 10.1016/j.ceramint.2014.01.122

Google Scholar

[10] Z. Luo, X.G. Zhou, J.S. Yu, K. Sun, F. Wang, Mechanical properties of SiC/SiC composites fabricated by PIP process with a new precursor polymer, Ceram. Intern. B40(2014)1939-(1944).

DOI: 10.1016/j.ceramint.2013.07.102

Google Scholar

[11] R. Jones, A. Szweda, D. Petrak, Polymer derived ceramic matrix composites, Composites: Part A 30(1995) 569-75.

DOI: 10.1016/s1359-835x(98)00151-1

Google Scholar

[12] C.L. Yan, R.J. Liu, Y.B. Cao, C.R. Zhang, Fabrication and properties of PIP 3D Cf/ZrC–SiC composites, Mater. Sci. Eng. A 591(2014)105-110.

DOI: 10.1016/j.msea.2013.10.102

Google Scholar

[13] Y.Z. Zhu, Z.R. Huang, S.M. Dong, M. Yuan, D.L. Jiang, The fabrication of 2D Cf/SiC composite by a modified PIP process using active Al powders as active filler, Mater. Characterization 59(2008)975-978.

DOI: 10.1016/j.matchar.2007.07.014

Google Scholar

[14] M.A. Schiavon, I.V.P. Yoshida, J.C. Bressiani, W. Acchar, Ceramic composites derived from polysiloxane/Al/Nb by AFCOP process, Adv. Powder Technol. 498–499 (2005) 375–380.

DOI: 10.4028/www.scientific.net/msf.498-499.375

Google Scholar