Microwave-Assisted Hydrothermal Synthesis of Mesoporous V-MCM-41 Materials with Good Hydrothermal Stability
Mesoporous V-MCM-41 materials with good hydrothermal stability had been synthesized by microwave-assisted hydrothermal method. The samples by microwave-assisted hydrothermal synthesis and conventional heating remain the same mesoporous structure by XRD and N2 adsorption analysis. The V-MCM-41 materials by microwave-assisted hydrothermal synthesis show the good hydrothermal stability, close to that of the materials by conventional heating. The high surface area of the sample by 720 W microwave treatment for 8 min was the same as that of the sample by conventional heating (110 °C for 12 h).
Zhong Cao, Lixian Sun, Xueqiang Cao, Yinghe He
J. Q. Xu et al., "Microwave-Assisted Hydrothermal Synthesis of Mesoporous V-MCM-41 Materials with Good Hydrothermal Stability", Advanced Materials Research, Vols. 233-235, pp. 1451-1454, 2011