A Systematic Investigation on the Preparation of 2, 6-Diamino-3, 5-Dinitropyridine
In this paper, the preparation of 2, 6-diamino-3, 5-dinitropyridine (DADNP) were systematically investigated. The optimal method was found. The key parameters have been systematically studied, such as the synthesis route, temperature, solvent, time, the reactant ratio, and the purification route. The optimal route was confirmed and would have an important reference for pilot plant scale-up.
Zhong Cao, Yinghe He, Lixian Sun and Xueqiang Cao
Y. H. Wang et al., "A Systematic Investigation on the Preparation of 2, 6-Diamino-3, 5-Dinitropyridine", Advanced Materials Research, Vols. 236-238, pp. 2299-2302, 2011