The Synthesis and Characterization of Nadic Dialkyl-Ester Derivatives with Trialkyl Borate

Yi Wen Jin; Jun Seong Park; Yong Sung Park; Je Wan Woo

doi:10.4028/www.scientific.net/AMR.415-417.1849

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The Synthesis and Characterization of Nadic Dialkyl-Ester Derivatives with Trialkyl Borate

Abstract:

In this study, nadic dialkyl-ester derivatives were synthesized via the reaction of nadic acid (NA) and trialkyl borate. Trialkyl borate was prepared by simple esterification of boric acid and a wide variety of alcohols. This synthesis process is a green process that does not use any solvent and catalysts. The boric acid can be recycled by filtration and can be used to prepare the trialkyl borate. The products were characterized by High-Performance Liquid Chromatography (HPLC) and Nuclear Magnetic Resonance (NMR).