Study on Crystal Structure and Thermal Stability of Hexaaquanickel (II) Bis[4-amino-3-methyl-benzenesulfonate]

Li Hua Wang

doi:10.4028/www.scientific.net/AMR.643.64

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 643Study on Crystal Structure and Thermal Stability...

Study on Crystal Structure and Thermal Stability of Hexaaquanickel (II) Bis[4-amino-3-methyl-benzenesulfonate]

Abstract:

Light green crystals of the Ni (II) complex material, [Ni(H2O)6](C14H16N2O6S2), were obtained by the self-assembly of Ni(H2O)6·6H2O, 4-amino-3-methyl-benzenesulfonic acid and NaOH. The result of X-ray diffraction shows that each Ni (II) atom is six-coordinated in a distorted octahedral environment by six oxygen atoms from the water molecules. The complex molecules are connected by hydrogen bonds to form two dimensional network structure. The thermal analysis shows that the complex has a enothermic peak at 302 C, indicating that coordinated water molecules are in the complex.

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Advanced Materials Research (Volume 643)

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64-67

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.643.64

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Online since:

January 2013

Authors:

Li Hua Wang

Keywords:

Analysis, Crystal Structure, Nickel (II) Complex, Thermal Stability

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References

[1] W.G. Lu, L. Jiang, X.L. Feng and T.B. Lu: Cryst. Growth Des. Vol. 6 (2006), p.564.

Google Scholar

[2] M.C. Hong: Cryst. Growth Des. Vol. 7 (2007), p.10.

Google Scholar

[3] G.M. Sheldrick: Program for X-ray crystal structure solution and refinement. Gottingen University, Germany, (1997).

Google Scholar

[4] K. Nakamota, Translated by Huang DR, Wang RQ. Infrand and Raman Spectra of Inorganic and Coordination Compounds. 3rd ed. Beijing: Chemical Industry Press(1986).

Google Scholar