Synthesis and Characterization of Silica-Lavender Microencapsulation by Sol Gel-Emulsion Method for Anti Mosquito Textile

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Microencapsulation is a new breakthrough in the field of nanotechnology that can be used for various applications, in particular for the application of controlled release material for functional textiles which were added by certain active substances and gave effects when used such as fragrance and anti mosquito textile. In this research, the synthesis of silica-lavender microencapsulation for anti-mosquito textile had been conducted successfully via sol-gel emulsion process. Sodium silicate solution which was emulsified into the lavender oil as an active ingredient acted as oil phase and ethanol solution acted as water phase. The addition of chitosan as surfactant and polymer for encapsulation with starch as soft template affected the rod-structure formation of nanorod. SEM result showed the morphology of silica-lavender. The rod has the average diameter size of 0.042-0.206 μm. The optimum result of rod-structure was obtained by adding 1% (v/v) of chitosan. FTIR analysis indicated the presence of absorbance peaks at wavenumber of 1411.89, 958.62, and 1078.2 cm-1 respectively for C-H (alkanes), C-H (alkenes) and ester functional groups which indicated the lavender compound in silica-lavender. UV-Vis analysis showed the maximum absorbance at wavelength of lavender at 350 nm. The combination of morphology and chemical properties of silica-lavender modified by chitosan-starch made this material as a candidate material for application in functional textile.

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215-218

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September 2013

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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