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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 789Synthesis and Characterization of Bacterial...

Synthesis and Characterization of Bacterial Cellulose-Based Carbon Nanotube by Catalytic Graphitization

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Abstract:

Bacterial cellulose-based carbon nanotube has been synthesized by catalytic graphitization method. Bacterial cellulose (BS) is a source of cellulose produced from fermentation of medium by Acetobacter xylinum. Since it contains unbranch polymer linked by β-1.4 glucopyronose with hydroxil groups, BS is able to use as precursor in synthesis of carbon nanotube. Due to catalytic graphitization, chitosan served as coupling agent and dispersant of catalyst and various concentration of catalyst FeCl3.6H2O also were used. Graphitization was conducted in furnace with inert nitrogen gas atmosphere at 800°C for 2 hours. SEM-EDS were used to evaluate the morphology and semi-quantitative analysis of sample. TEM was used to determine the microstructures and crystallographic. When the chitosan was added 0.5%, its served as coupling agent and dispersant of catalyst with BS. Chitosan improved physical properties, relieved its brittleness, and caused the optical properties of BS. Catalyst of FeCl3.6H2O was used to assist the formation and growth of carbon nanotube. The amount of carbon was not affected by time aging. 0.1 M FeCl3.6H2O was the optimum concentration to produce carbon nanotube with 81, 58% the mass of carbon, plane orientation (002) (100) and the diameter of carbon nanotube is 25 nm.

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Advances in Materials, Processing and Manufacturing

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Periodical:

Advanced Materials Research (Volume 789)

Pages:

232-236

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.789.232

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Online since:

September 2013

Authors:

Elsy Rahimi Chaldun, Myrtha Karina, Bambang Sunendar Purwasasmita

Keywords:

Bacterial Cellulose, Catalytic Graphitization, Chitosan, FeCl3.6H2O, Graphite

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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[1] I. Sirὀ, D. Plackett: Cellulose. Vol. 17 (2010), pp: 459-494.

[2] L. Indrarti dan Indriyati: Teknologi IndonesiaVol. 34. No. 1 (2011), pp: 16-22.

[3] C. Gao, Y. Wan,C. Yang, K. Dai • T. Tang • H. Luo, J. Wang. Preparation and characterization of bacterial cellulose spongewith hierarchical pore structure as tissue engineering scaffold : J. Porous Mater, Springer (Published online 20 Februari 2010).

DOI: 10.1007/s10934-010-9364-6

[4] K. Wojciech, T. t. Czaja, David, J. Young, T.M. Kawecki, § and R. Malcolm Brown, Jr: Biomacriomolecules. Vol 8, No 1 (2007), pp.1-12.

[5] A. Rezaee, H. Godini , H. Bakhtou : Environmental Engineering and Management Journal. Vol. 7, No. 5 (2008), pp: 589-594. J. Porous Material, Published online 20 February (2010).

[6] S.H. Yoon, H.J. Jin, M.C. Kook, and Y.R. Pyun: BiomacromoleculesVol. 7. No 4 (2006), pp: 1280-1284.

[7] L. Indrarti , R. Yudianti, K. Amurwabumi, and N. Yuli: Indonesian Journal of Biotechnology (1998).

[8] L. Indrarti, R. Yudianti, K. Amurwabumi. 2001. Loudspeaker Membrane from Nata de coco, Cocoinfo International Magazine. Vol. 8: 1 (2001), pp: 15-16.

[9] L. Indrarti, E. Rahimi : National Proceeding of Food (2008), ISBN 978-979-95554-4-1.

[10] Indriyati, et. al. 2006. Modification bioselulosa (Nata de coco) for backing layer of Fuel Cell. (Research repot, Research Center for Physics, Indonesian Institute of Sciences, 2006).

[11] H. Onggo: Fabricating Conductive biocelullose forgas diffusion layer, (Research report, Research Center for Physics, Indonesian Institute of Sciences, pp: 2-3, 2009).

[12] S. Yamanaka , K. Watanabe, N. Kitamura, M. Iguchi, S. Mitsuhashi, Y. Nishi, M. Uryu: Journal of Material Science Vol. 24 (1989), pp: 3141-3145.

DOI: 10.1007/bf01139032

[13] L. Indriyati, E. Rahimi: Indonesian Material Sciences Journal , Vol. 8 (2006), pp: 40-44.

[14] A. Oya and H. Marsh: Journal of Material Science(1982), pp.309-322.

[15] H. Marsh , D. Crawford , DW. Taylor : Carbon Vol. 21: 1 (1983); pp: 81-7.

[16] F.J. Maldonado-Hodar, C. Moreno-Castilla , J. Rivera-Utrilla, Y. Hanzawa, Y. Yamada: Langmuir Vol 16: 1(2001), pp: 4367-73.

DOI: 10.1021/la991080r

[17] S. Han , Y. Yun Y, K. W Park, Y.E. Sung, T. Hyeon: Adv Mater Vol. 15: 22 (2003), pp: 1922-5.

[18] Sevilla M, Fuertes AB. Carbon 44: 3. (2006). pp: 468-74.

[19] M. Ul-Islam, N. Shah, J.H. Ha, J.K. Park: Korean J. Chem. Eng (2011), pp: 1736-1742.

[20] Information on http: /www. mpilkington. com/Lecture_29. pdf M. Pilkington, "Prinsiples of inorganic chemistry.

[21] Kenneth B.K. Teo: Encyclopedia of Nanosience and Nanotechnology. Vol.X. (2003). p: 1-22.