Synthesis and Hydrogen Absorption Capacity of Multilayered SnO2 Hollow Microspheres

Zhi Yuan Wang; Feng Ping Wang; Ming Yan Li; M. Zubair Iqbal; Qurat Ul Ain Javed; Yan Zhen Lu; Mei Xu; Quan Shui Li

doi:10.4028/www.scientific.net/AMR.924.57

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 924Synthesis and Hydrogen Absorption Capacity of...

Synthesis and Hydrogen Absorption Capacity of Multilayered SnO₂ Hollow Microspheres

Abstract:

Multilayered SnO₂ hollow microspheres (MHS-SnO₂) have been successfully synthesized via a solvothermal method by using glycol-water as solvent. The morphology, composition and structure of the product have been characterized by field-emission scanning electron microscopy (FESEM) with an energy dispersive X-ray (EDX) spectroscopy, transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM) with selected area electron diffraction (SAED) and X-ray diffraction (XRD). The FESEM, TEM and HRTEM images indicate that the as-prepared microspheres show multilayered structure and the wall of the hollow microspheres is composed of single crystalline nanoparticles. Study on hydrogen absorption characteristics of MHS-SnO₂ performed at 373 K shows a good absorption capacity of 0.85 wt.%.

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Periodical:

Advanced Materials Research (Volume 924)

Pages:

57-60

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.924.57

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Online since:

April 2014

Authors:

Zhi Yuan Wang, Feng Ping Wang*, Ming Yan Li, M. Zubair Iqbal, Qurat Ul Ain Javed, Yan Zhen Lu, Mei Xu, Quan Shui Li

Keywords:

Hydrogen Absorption, SnO₂, Solvothermal

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