Synthesis of Aminotriacetic Acid Intercalated MgAl-Layered Double Hydroxides and its Selective IR Absorption Properties

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A novel aminotriacetic acid (NTA) intercalated MgAl-LDHs have been successfully synthesized by anion exchange method with MgAl-NO3-LDHs as precursor. The XRD pattern implies that NTA anions have replaced NO3- in the interlayer of LDHs. The FT-IR spectra also indicates that NTA anions have intercalated into layers’ space of LDHs, and the carboxyl groups of NTA have been converted into carboxyl anions after intercalation process. When comparing IR spectra of MgAl-NTA-LDHs and MgAl-CO3-LDHs, higher and stronger absorption was observed in the range of 1428-1250 cm-1, especially in the range of 1111-909 cm-1.

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33-37

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August 2014

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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