Key Engineering Materials
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Key Engineering Materials Vols. 342-343
Paper Title Page
Abstract: Rod shaped nanocrystalline powders of hydroxyapatite (HAp) were synthesized by a low
temperature chemical route involving calcium nitrate tetrahydrate and sodium phosphate. Three
types of alkyl ammonium bromide surfactants i.e. tetrapropylammonium bromide,
tetraethylammonium bromide and tetramethylammonium bromide were used to regulate the
nucleation and crystal growth. The synthesized powders were characterized by XRD, SEM and FTIR.
The effect of the various alkyl ammonium bromide surfactants on the phase formation, particle
size and morphology of the hydroxyapatite powders has been investigated and reported.
873
Abstract: Nanosized hydroxyapatite(HAp) was synthesized hydrothermally and influence of
processing parameters, such as reaction temperature and time, pH, and Ca/P ratio, on the phase
stability of HAp was evaluated after pressureless sintering at 1250°C in air. The highest stability
was achieved from the powder obtained at a processing condition for the lowest solubility of Ca2+,
which corresponds to temperature close to 200°C, time <4h, pH>9.0, and Ca/P = 1.67. The stability
of nanosized HAp in HAp/3Y-TZP composites was slightly inferior to commercial one, but the
involvement of hydrothermally synthesized HAp improved sintered density of the composites and
stability of t-ZrO2 phase in the composites.
877
Abstract: Various studies recommend that threaded type implants should be used to maximize
initial contact, improve initial stability, enlarge implant surface area, and favor dissipation of
interfacial stress. The objective of this study was to compare four types of screw implants placed in
posterior region of mandible model and evaluate the influences of implant shape, configuration,
length, diameter and abutment connection method on stress distribution using a three-dimensional
finite analysis. Four types of two-length implant models — 8.5 and 13 mm — were selected and the
wide diameter was also used. Four groups were classified by implant outline and connection
manner A load of 100 N was applied vertically on the center of the implant. Oblique and horizontal
loads were taken as equal to that of the vertical load. The TMJ area in mandibular model was
constrained in all directions. Results show that the stress of two-length implants was similar in all
groups and the internal connection implant with appropriate thickness of inner part of the implant
had better stress distribution.
885
Abstract: Plastic substrates were modified with 2-methacryoyloxyethyl phosphorylcholine (MPC) copolymer
brushes by surface-initiated atom transfer radical polymerization (ATRP) with a mean chain density
of 2.44 chains/nm2 and a chain length around 50nm. Ellipsometry, X-ray photoelectron
spectroscopy, gel permeation chromatography, nuclear magnetic resonance and atomic force
microscopy were used to characterize the modified surfaces.MPC was copolymerized with a
methacrylate monomer including an active ester unit which can link covalently with antibodies.
They latter were immobilized on these well-defined surfaces for characterization and a further use
in enzyme-linked immunosorbent assay (ELISA).All kinds of surfaces displayed a good density of
immobilized antibodies mainly forming globular packs of around 500 units. A water-soluble MPC
polymer-based stabilizer added to the antibody solution could further their individual
immobilization.
889
Abstract: The 2% NaF and 8% SnF2 have been used in topical fluoridation method in the dental
office to increase the resistance of enamel to acid dissolution. Bis-GMA based monomers have been
used for the basic materials in the dental pit and fissure sealants. Therefore, the resinous pit and
fissure sealant including fluorides may increase the effect of preventing dental caries. In this study,
we made a novel dental pit and fissure sealant and evaluated some properties, especially fluoride
release. In order to make experimental pit and fissure sealant including fluoride, NaF and SnF2
powder were added into self-made monomer composed of Bis-GMA, TEGDMA, UDMA and photo
initiator system by weight percent of 2% and 8% respectively. The just monomer without fluoride
powder was used for control. Uncured film thickness and depth of cure were measured according to
ISO specification 6874:1988 and the viscosity was measured using rheometer. The five disc
specimens were made using light curing unit to evaluate fluoride releasing and each specimen was
immersed in the artificial saliva of 10 mL. Fluoride ion concentrations in extracts were measured
for 3 days using fluoride electrode at every 12 hrs. There was no significant difference between
experimental and control group in the depth of cure, uncured film thickness, and viscosity (p>0.05).
The released fluoride ion concentration was continuously retained for 72 hrs.
893
Abstract: The hybrid Silver(Ag) nanoparticles were synthesized by gamma-irradiation, and
characterized by field-emission transmittance electron microscopy (FE-TEM), field-emission
scanning electron microscopy (FE-SEM), and energy dispersive X-ray spectroscopy (EDXS). The
electron microscopy images show that well-dispersed Ag nanoparticles of about 3-7 nm were
loaded to the outer and inner side of SiO2 nanoparticles of about 5-30 nm. Antifungal efficiency of
the hybrid nanoparticles was tested against Aspergillus flavus ATCC 64025, Aspergillus fumigatus
ATCC 16424, Aspergillus terreus ATCC 46941, Candida albicans ATCC 10231, Candida albicans
A207(clinical isolate), Candida glabrata ATCC 48435, Candida krusei ATCC 6258, Candida
lusitaniae ATCC 42720, Candida parapsilosis ATCC 34136, Candida tropicalis ATCC 13803,
Cryptococcus neoformans ATCC 36556, and Mucor ramosissmus ATCC 90286. At the presence of
hybrid Ag nanoparticles at 1 ppm, they did not grow fully even after 58 hrs except for Cryptococcus
neoformans ATCC 36556. The hybrid Ag nanoparticle can be used for antifungal agents.
897
Abstract: In order to evaluate the mechanical properties of the human skeletal muscles, the
elasticity and viscosity of the human calf muscles were measured with Magnetic Resonance
Elastography (MRE). MRE is a novel method to measure the mechanical properties of living soft
tissues in vivo quantitatively by observing the strain waves propagated in the object. In this study,
the shear modulus and viscosity coefficient were measured with MRE. The shear modulus was 3.7
kPa in relaxed state, and increased with increasing the muscle forces. Interestingly, the viscosity
was changed with the vibration frequency applied to the muscles, that was 4.5 Pa·s at 100Hz
vibration and 2.4 Pa·s at 200Hz vibration. This shows clearly the visco-elastic property.
901
Abstract: Tissue-engineering must be either manufactured aseptically or sterilized after processing.
To extend protection of medical devices against microbial contamination, various sterilization
methods have been suggested. Hydrogen peroxide gas plasma sterilization has been applied in
hospitals worldwide for almost a decade. In this study, we investigated the sterilization efficacy of
hydrogen peroxide gas plasma sterilizer with porous polyurethane sample. The result is suggested
that hydrogen peroxide gas plasma can be applicable to the sterilization of polymer scaffold for
tissue engineering materials.
905
Abstract: Osseointegration (OI) could be described as the modality for stable fixation of titanium
implant to bone structure. The OI has become a realized phenomenon of importance in the dental
and rehabilitation sciences since recently developed dentures and artificial limbs are directly
attached to human skeleton by using osseointegrated implants. Previously, a study showed that bone
strain generated potential (SGP) that is an electrical potential and considered to be generated by
fluid flow in bone could be used as a parameter to examine the amount of OI on implant-bone
interface. SGP generation is known to require intraosseous fluid flow related with generations of
pore pressure gradient in bone. Therefore, SGP would interact with properties determining
interstitial fluid flow characteristics such as viscosity, velocity, flow path directions, and interstitial
fluid flow boundary conditions. Since interstitial fluid flow characteristics in bone are governed by
pore pressure gradient, it could be possible to predict SGP indirectly through the prediction of pore
pressure generation in bone. The aim of this study is to predict the distribution of pore pressure in
OI bone-implant composite representing a completely osseointegrated rabbit tibia-titanium implant
composite. The theoretical background of this prediction is based on the poroelasticity of 2-phase
material that grounds on fluid flow and behavior of cortical bone material. In this study, we
constructed a finite element (FE) model of the composite from images of micro-CT scanning. In the
next step, we examined analysis of the FE model about pore pressure by using ABAQUS. In this
analysis, the constitutive behavior was externally computed by utilizing a user subroutine. The
results showed the different spatial distributions of pore pressure in the composite. The magnitudes
of pore pressure were found to be significantly increased when the position was approached for the
interface of implant-bone. Further analytical study is required to fully understand relationships
between SGP and pore pressure distributions in OI bone-implant composite materials.
909