Hydrothermal Synthesis of Nano-Structured Barium Titanate from Metatitanic Acid

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Abstract:

Nano-structured Barium Titanate (BaTiO3) was prepared by a hydrothermal method with the reaction between metatitanic acid and an alkaline solution of Ba(OH)2•8H2O. The morphology of as-obtained powders of BaTiO3 was determined by Scanning Electron Microscope, which revealed that well-dispersed nanoparticles were successfully synthesized. The phase composition was analyzed by X-ray diffraction, which shows that cubic phase of Barium Titanate was prepared. The optimal reaction conditions were discussed in detail.

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Key Engineering Materials (Volumes 434-435)

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311-313

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March 2010

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© 2010 Trans Tech Publications Ltd. All Rights Reserved

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[1] X.H. Wang, R.Z. Chen, H. Zhou, et al.: Ceram. Inter. Vol. 30 (2004), P. 1895.

Google Scholar

[2] M.T. Buscaglia, V. Buscaglia, M. Viviani, et al.: J. Am. Ceram. Soc. Vol. 84 (2001), p.376.

Google Scholar

[3] C.L. Chen, Y. l. Wei, X. l. Jiao, et al.: Mater. Chem. Phys. Vol. 110 (2008), p.186.

Google Scholar

[4] C.K. Tan, Goh and K.L. Gregory: Thin Solid Films. Vol. 515 (2007), p.6572.

Google Scholar

[5] X.H. Wang, R.Z. Chen, Z.L. Gui, et al. Mater. Sci. Eng. B Vol. B99 (2003), p.199.

Google Scholar

[6] E. Brzozowski and M. S. Castro, J. Eur. Ceram. Soc. Vol. 20 (2000), p.2347.

Google Scholar

[7] J.M. Zeng, C.L. Lin, J.H. Li, et al.: Mater. Lett. Vol . 38 (1999),P. 112-115.

Google Scholar

[8] H. Matsuda, N. Kobayashi, T. Kobayashi, et al.: J Non-Crystal. Sol. Vol. 271(2000), p.162.

Google Scholar

[9] H. Kumazawa and K. Masuda, Thin Solid Films. Vol. 353 (1999), p.144.

Google Scholar

[10] X. Wei, G. Xu, Z.H. Ren, et al.: Mater. Lett. Vol. 62 (2008), p.3666. Fig 2. A typical SEM image of nano-structured BaTiO3 synthesized by hydrothermal reaction.

Google Scholar