Effect of Milling Time on Properties of Ti-48at%Al Composite Powder Prepared by High Energy Milling

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Abstract:

The Ti-48at%Al composite powder was synthesized by high energy ball milling. The properties of the composite particles, such as medium diameter,Phase ,microstructure and components, were respectively investigated . Results show that, the phase evolution process can be described by: Ti+ Al fcc Ti (Al),TiAl,TiAl3,Ti3AlTiAl3,Ti3Alamorphous phase. After milling 3 hours, Fcc Ti (Al) solid solution, TiAl, TiAl3, Ti3Al were found. After milling 9 hours, the amorphous phase of Ti - 48 at % Al were produced. The element distribution of the mechanically alloyed Ti-48at%Al powder was close to the initial design composition after 5 h milling, but this distribution was inhomogeneous. Medium diameter (D50) of Ti-48at%Al composite powder achieved the minimal size 9.56 μm after milling for 5hours.

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Key Engineering Materials (Volumes 609-610)

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185-190

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April 2014

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] Skrotzki B. A New Microstructural View of Creep in Near-γ TiAl-Alloys[J]. Key Engineering Materials, 1999, 171: 701-708.

DOI: 10.4028/www.scientific.net/kem.171-174.701

Google Scholar

[2] Xu J H, Fu Y C, Ge Y F. Experimental Study on High Speed Milling of γ-TiAl Alloy[J]. Key Engineering Materials, 2007, 339: 6-10.

DOI: 10.4028/www.scientific.net/kem.339.6

Google Scholar

[3] Silva C R M, Henriques V A R. Production of titanium alloys for medical implants by powder metallurgy[J]. Key Engineering Materials, 2001, 189: 443-448.

DOI: 10.4028/www.scientific.net/kem.189-191.443

Google Scholar

[4] Bhattacharya P, Bellon P, Averback R S, et al. Nanocrystalline TiAl powders synthesized by high-energy ball milling: effects of milling parameters on yield and contamination[J]. Journal of Alloys and Compounds, 2004, 368(1): 187-196.

DOI: 10.1016/j.jallcom.2003.08.079

Google Scholar

[5] Gebhard S, Pyczak F, Göken M. Microstructural and micromechanical characterisation of TiAl alloys using atomic force microscopy and nanoindentation[J]. Materials Science and Engineering: A, 2009, 523(1): 235-241.

DOI: 10.1016/j.msea.2009.05.068

Google Scholar

[6] Appel F, Oehring M, Paul J D H. A novel in situ composite structure in TiAl alloys[J]. Materials Science and Engineering: A, 2008, 493(1): 232-236.

DOI: 10.1016/j.msea.2007.08.095

Google Scholar

[7] Kim Y W. Ordered intermetallic alloys, part III: gamma titanium aluminides[J]. Jom, 1994, 46(7): 30-39.

DOI: 10.1007/bf03220745

Google Scholar

[8] Kim Y W. Intermetallic alloys based on gamma titanium aluminide[J]. Jom, 1989, 41(7): 24-30.

DOI: 10.1007/bf03220267

Google Scholar

[9] Wenbin F, Lianxi H, Wenxiong H, et al. Microstructure and properties of a TiAl alloy prepared by mechanical milling and subsequent reactive sintering[J]. Materials Science and Engineering: A, 2005, 403(1): 186-190.

DOI: 10.1016/j.msea.2005.04.049

Google Scholar

[10] Lu L, Lai M O, Froes F H. The mechanical alloying of titanium aluminides[J]. JOM, 2002, 54(2): 62-64.

DOI: 10.1007/bf02701079

Google Scholar

[11] Djanarthany S, Viala J C, Bouix J. An overview of monolithic titanium aluminides based on Ti3Al and TiAl[J]. Materials Chemistry and Physics, 2001, 72(3): 301-319.

DOI: 10.1016/s0254-0584(01)00328-5

Google Scholar

[12] Zhang F, Lu L, Lai M O, et al. Grain growth and recrystallization of nanocrystalline Al3Ti prepared by mechanical alloying[J]. Journal of materials science, 2003, 38(3): 613-619.

Google Scholar

[13] Suryanarayana C. Mechanical alloying and milling[J]. Progress in materials science, 2001, 46(1): 1-184.

Google Scholar

[14] Zhang D L. Processing of advanced materials using high-energy mechanical milling[J]. Progress in Materials Science, 2004, 49(3): 537-560.

DOI: 10.1016/s0079-6425(03)00034-3

Google Scholar

[15] LI X, SUN H, FANG W, et al. Structure and morphology of Ti-Al composite powders treated by mechanical alloying[J]. Transactions of Nonferrous Metals Society of China, 2011, 21: s338-s341.

DOI: 10.1016/s1003-6326(11)61602-6

Google Scholar

[16] Zhang fu bang, Cheng xue ding, Hao lei et al. Co80Zr20 amorphous alloy powder prepared by mechanical alloying[J]. Powder Metallurgy Technology, 2006, 24(5): 340-344.

Google Scholar