Repeatability in Rheological Measurements of Epoxy Resin

Liu Ying Huang; Hong Yu Wang; Xuan Cheng; Ying Zhang

doi:10.4028/www.scientific.net/KEM.768.64

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HomeKey Engineering MaterialsKey Engineering Materials Vol. 768Repeatability in Rheological Measurements of Epoxy...

Repeatability in Rheological Measurements of Epoxy Resin

Abstract:

Shear stress-shear strain rate and shear stress-shear time curves of epoxy resin samples with the number average molecular weight of 283 g/mol were measured at 50 °C under the modes of steady test and transient test, respectively. Effects of dealy time (t₁) and measurement time (t₂) on the shear stress-shear responses of the epoxy resin oligomer material were studied. It was found that the repeatability of the test results at small shear rates was significantly influenced by the delay time and the measurement time. The values of t₁ and t₂ parameters to be used for the steady test of epoxy resin oligomer material could be optimized based upon the transient test. The measurement repeatablity at shear rates smaller than 7 s^-1 was apparently improved by setting the delay time and the measurement time longer than 20 s seperately (t₁³ 20 s, t₂³ 20 s) with the total delay time and the measurement time shorter than 80 s (t₁+ t₂ £ 80s).

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Periodical:

Key Engineering Materials (Volume 768)

Pages:

64-68

DOI:

https://doi.org/10.4028/www.scientific.net/KEM.768.64

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Online since:

April 2018

Authors:

Liu Ying Huang, Hong Yu Wang, Xuan Cheng, Ying Zhang*

Keywords:

Epoxy Resin, Repeatability, Steady Test, Transient Test

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References

[1] ARES user manual, TA Instruments—Waters LLC, New Castle, (2003).

Google Scholar

[2] X. Cheng, X. W. Bai, J. J Li, H. Z. Chen, Y. Zhang. Experimental Observations of Time-dependent Behaviors for Polycarbosilane Melt. Journal of Applied Polymer Science, 120, (2011), 3395-3400.

DOI: 10.1002/app.33299

Google Scholar

[3] L. Y. Huang, Z. Q. Zhu, X. Cheng, Y. Zhang. Rheological Measurement of In Situ Preheating Polycarbosilane Melt. Key Engineering Materials, 726, (2017), 90-94.

DOI: 10.4028/www.scientific.net/kem.726.90

Google Scholar

[4] Z. Q. Zhu, L. Y. Huang, X. Cheng, Y. Zhang, Determining Zero Shear Viscosity of Polycarbosilane Melts, Key Engineering Materials, 726, (2017), 95-99.

DOI: 10.4028/www.scientific.net/kem.726.95

Google Scholar