Binder Based Processing of Magnesium Alloy WE43 towards Biomedical Application Using Metal Injection Molding (MIM)

Article Preview

Abstract:

In this study to the authors knowledge 1st time, Metal Injection Molding (MIM) technique was used to introduce the magnesium alloy WE43 into binder-based powder metallurgical (PM) processing. Towards later adoption to binder-based 3D-printing technologies, Fused Granular Fabrication (FGF) technique, respectively for biomedical application. Metal Injection Moulding (MIM) is a binder based economic near net shape prototyping technique for production of complex shaped parts in high number and high reproducibility, and hence perfect as a “gold standard” for the introduction of new Mg-alloys into binder passed PM processing. In doing so, dogbone shape tensile test specimen were manufactured by MIM, subsequently solvent debound and conventional sintered in argon atmosphere. Next to the as sintered specimens (asS), solid solution heat treatment (T4) and precipitation hardening heat treatment (T6) were performed on additional specimens. Tensile tests pointed out high strength and ductility of as sintered and heat treaded specimens of up to 226 MPa UTS at 7.6% elongation at fracture. The microstructure was investigated using SEM imaging technique equipped with energy disperse x-ray energy analysis (EDX) for secondary phase analysis. Hence, the magnesium alloy WE43 could be identified as a high strength and ductility alloy for binder based PM processing for future additive manufacturing approaches in biomedical applications of patient adapted implants.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

157-163

Citation:

Online since:

December 2023

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2023 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] M. Wolff, J. G. Schaper, M. R. Suckert, M. Dahms, F. Feyerabend, T. Ebel, R. Willumeit-Römer, T. Klassen, Metal Injection Molding - MIM of Magnesium and its Alloys, Metals, Vol.6 No.118 (2016), DOI:10.3390/ met 6050118.

DOI: 10.3390/met6050118

Google Scholar

[2] J. G. Schaper, M. Wolff, B. Wiese, T. Ebel, R. Willumeit-Römer, Powder Metal Injection Moulding and Heat Treatment of AZ81 Mg Alloy, JMPT, Vol.267 (2018) 241-246.

DOI: 10.1016/j.jmatprotec.2018.12.015

Google Scholar

[3] M. Wolff, M. Dahms, T. Ebel. Sintering of Magnesium, Advanced Engineering Materials 12 (2010) 829-836.

DOI: 10.1002/adem.201000038

Google Scholar

[4] M. Wolff, H. Helmholz, M. Luczak, D. Strerath, T. Ebel, R. Willumeit-Römer, In Situ X-ray Synchrotron Radiation Analysis, Tensile- and Biodegradation Testing of Redox-Alloyed and Sintered MgCa-Alloy Parts Produced by Metal Injection Moulding, Metals (2022) 12, 353.

DOI: 10.3390/met12020353

Google Scholar

[5] M. Wolff, S. Klahn, H. Buresch, T. Ebel, R. Willumeit-Römer, MIM and Binder based 3D-printing Approach of High Strength Magnesium Alloy Mg-6.3Gd, World PM2022 Proceedings, (2022).

Google Scholar

[6] W. Ali et al, Bioabsorbable WE43 Mg alloy wires modified by continuous plasma-electrolytic oxidation for implant applications. Part I: Processing, microstructure and mechanical properties Biomaterials Advances Volume 146, March 2023, 213314, https://doi.org/10.1016/j.bioadv. 2023.213314

DOI: 10.1016/j.bioadv.2023.213314

Google Scholar

[7] L. Li et al, Corrosion, mechanical and biological properties of biodegradable WE43 alloy modified by Al ion implantation, Ceramics International Volume 49, Issue 3, 1 February 2023, Pages 5327-5334.

DOI: 10.1016/j.ceramint.2022.10.056

Google Scholar

[8] https://www.syntellix.de/en/products/technology.html

Google Scholar

[9] Cengiz, I.F., Oliveira, J.M. & Reis, R.L. Micro-CT – a digital 3D microstructural voyage into scaffolds: a systematic review of the reported methods and results. Biomater Res 22, 26 (2018)

DOI: 10.1186/s40824-018-0136-8

Google Scholar

[10] H.S. Jiang et al, Microstructure and mechanical properties of WE43 magnesium alloy fabricated by direct-chill casting, Materials Science & Engineering A, Volume 684, 27 January 2017, Pages 158-164.

DOI: 10.1016/j.msea.2016.11.009

Google Scholar

[11] Nayeb-Hashemi AA, Phase Diagrams of Binary Magnesium Alloys, ASM International, Metals Park, Ohio, USA, (1998)

Google Scholar

[12] https://www.azom.com/article.aspx?ArticleID=8539

Google Scholar