Investigation on Biocompatibility and Mechanical Properties of Ti15Mg Alloy

Article Preview

Abstract:

In this research work, bioactive Ti15Mg alloy was prepared by powder metallurgy route to investigate its biocompatibility and mechanical properties. Many tests were performed including X-ray diffraction; optical microscope analysis, scanning electron microscope analysis, ultrasonic wave test, corrosion behavior test, Static immersion test, and the wet sliding wear test. The XRD result shows that the prepared alloy sample consist of (α-Ti phase) and Mg. The microstructure of the prepared alloy sample consisted of a biodegradable Mg or pore and alpha titanium. The effect of the Mg content on degradability was tested based on simulated body fluid of Ringer solutions using electrochemical corrosion. The findings indicate that an elastic modulus of 47GPa exhibits the alloy. There were low corrosion rates of the alloy. The Ti matrix remained integrity after 14 days of immersion in the Ringer solutions, and the magnesium phase dissolved in the solution, causing a layer to form on the alloy. The wear behavior of the prepared ally at wet sliding conditions was evaluated using pin on disc method. The in vitro analysis showed good biocompatibility with Ti15Mg alloy. The prepared alloy demonstrates good biocompatibility and bioactivity.

You might also be interested in these eBooks

Info:

Periodical:

Materials Science Forum (Volume 1039)

Pages:

557-564

Citation:

Online since:

July 2021

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2021 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] P. Lichte, H. C. Pape, T. Pufe, P. Kobbe, & H. Fischer, Scaffolds for bone healing: concepts, materials and evidence. Injury, 42(6) (2011) 569-573.

DOI: 10.1016/j.injury.2011.03.033

Google Scholar

[2] J. M. Anderson, A. Rodriguez & D. T. Chang, Foreign body reaction to biomaterials, In Seminars in immunology (Vol. 20, No. 2, (2008) pp.86-100, Academic Press.

DOI: 10.1016/j.smim.2007.11.004

Google Scholar

[3] R. Narayan, ASM Hand book, Volume 23, Materials for Medical Devices. Materials Park: ASM International. (2012).

Google Scholar

[4] B.V. Krishna, S. Bose, A. Bandyopadhyay, Low stiffness porous Ti structures for load-bearing implants, Acta Biomater. 3 (2007) 997-1006.

DOI: 10.1016/j.actbio.2007.03.008

Google Scholar

[5] Z. Esen, B. Dikici, O. Duygulu, A.F. Dericioglu, Titanium–magnesium based composites: Mechanical properties and in-vitro corrosion response in Ringer's solution, Mater. Sci. Eng. A 573 (2013) 119-126.

DOI: 10.1016/j.msea.2013.02.040

Google Scholar

[6] M.P. Staiger, A.M. Pietak, J. Huadmai, G. Dias, Magnesium and its alloys as orthopedic biomaterials: a review, Biomaterials 27 (2006) 1728-1734.

DOI: 10.1016/j.biomaterials.2005.10.003

Google Scholar

[7] N.T. Kirkland, Magnesium biomaterials: past, present and future, Corrosion Engineering, Sci. Tech. 47 (2012) 322-328.

DOI: 10.1179/1743278212y.0000000034

Google Scholar

[8] O. Duygulu, A.A. Kaya, G. Oktay, F.C. Sahin, Diffusion bonding of magnesium, zirconium and titanium as implant material, Mater. Sci. Forum 546–549 (2007) 417–420.

DOI: 10.4028/www.scientific.net/msf.546-549.417

Google Scholar

[9] M. Qian, F.H. Froes, Titanium Powder Metallurgy: Science, Technology and Applications, Elsevier Science (2015) ISBN: 9780128009109.

Google Scholar

[10] Haydar Al-Ethari, Sundus Abbas, Ekhlas Khalid Zamel, optimization of Manufacturing Titanium-Magnesium Alloy for Biomaterial Applications Using Grey Relational Analyses, 1st International Conference on Engineering Sciences: INTCSET 2020, will be published in the Journal of Material Sciences and Engineering: IOP Conference Series.

DOI: 10.1088/1757-899x/1094/1/012148

Google Scholar

[11] H. Al-Ethari, A.H. Haleem, and N.M. Gased, IOP Publishing.May, An Investigation on Chemical Machining of NiTi SMA Prepared by Powder Metallurgy. In IOP Conference Series: Materials Science and Engineering (Vol. 518, No. 3, 2019, p.032032).].

DOI: 10.1088/1757-899x/518/3/032032

Google Scholar

[12] A. H. Jaafar, & H. Al-Ethari, Numerical and experimental investigations of cutting force for NAB-CBN composite. The Iraqi journal for mechanical and materials engineering, 18(4), (2018) 589-603.

DOI: 10.32852/iqjfmme.v18i4.231

Google Scholar

[13] Jaafar, A. H., & Al-Ethari, H. (2018). NUM ERICAL AND EXPERIMENTAL INVESTIGATIONS OF CUTTING FORCE FOR NAB-CBN COMPOSITE. THE IRAQI JOURNAL FOR MECHANICAL AND MATERIALS ENGINEERING, 18(4), 589-603].

DOI: 10.32852/iqjfmme.v18i4.231

Google Scholar

[14] Sarah Muhi Jawad, Effect of (Cu & Cr) Additives on Corrosion and Dry Sliding Wear of NiTi Shape Memory Alloy, MSC thesis, Submitted to the Council of the College of Materials engineering / University of Babylon], (2015).

Google Scholar

[15] I. Mutlu, and E.Oktay, Characterization of 17-4 PH stainless steel foam for biomedical applications in simulated body fluid and artificial saliva environments, Materials Science and Engineering: C, Vol. 33, No. 3, (2013) pp.1125-1131.

DOI: 10.1016/j.msec.2012.12.004

Google Scholar

[16] G. K. Meenashisundaram, N.Wang, S., Lu, S. Maskomani, S. K. Anantharajan, S. T. Dheen, & J. Wei, Fabrication of Ti+ Mg composites by three-dimensional printing of porous Ti and subsequent pressureless infiltration of biodegradable Mg. Materials Science and Engineering: C, 108, (2020), 110478.

DOI: 10.1016/j.msec.2019.110478

Google Scholar

[17] D.Kuroda, H. Kawasaki, S. Hiromoto, & T. HANAWA, (2005) Annual Book of ASTM Standards, Section 13, Medical Devices and Services Annual Book of ASTM Standards, Section 13, Medical Devices and Services, 2000, Materials transactions, 46(7), 1532-1539.

DOI: 10.1097/00149078-198806010-00014

Google Scholar

[18] P. J. Leonard-Mayer, A surface resistivity method for measuring hydrologic characteristics of jointed formations (Vol. 8901), US Department of the Interior, Bureau of Mines (1984).

Google Scholar

[19] Y.‏ Okazaki, & E. Gotoh, Comparison of metal release from various metallic biomaterials in vitro. Biomaterials, 26(1), (2005) 11-21.

DOI: 10.1016/j.biomaterials.2004.02.005

Google Scholar

[20] S. Ouyang, Y.Liu, Q., Huang, Z., Gan, & H. Tang, Effect of composition on in vitro degradability of Ti–Mg metal-metal composites. Materials Science and Engineering: C, 107, 110327, (2020).

DOI: 10.1016/j.msec.2019.110327

Google Scholar

[21] Z. Esen, B. Dikici, O. Duygulu, and A.F. Dericioglu, Titanium–magnesium based composites: mechanical properties and in-vitro corrosion response in Ringer's solution. Materials Science and Engineering: A, 573, (2013) pp.119-126.

DOI: 10.1016/j.msea.2013.02.040

Google Scholar

[22] D. F. Williams, Biocompatibility of Clinical Implant Mtls. CRC-Press, (1981).

Google Scholar