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A Preliminary Study of Isolation and Characterization of Nanocrystalline Cellulose from Microcrystalline Cellulose by Acid Hydrolysis Process

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Abstract:

This research focuses on the isolation of MCC (microcrystalline cellulose) into NCC (nanocrystalline cellulose) by acid hydrolysis process. The sulfuric acid hydrolysis (44 wt.% H2SO4) aims to fibrillation from MCC into NCC material. NCC has good properties such as high-surface-area, high-aspect-ratio, weight light, and reactive materials. The morphology of NCC was characterized by SEM (Scanning Electron Microscope) and TEM. The physical characterization was tested using FTIR, XRD, and TGA. The morphological result showed that the particle size of NCC was more homogeneous with a diameter size of 25±3 nm with 310±5 nm in length. The physical properties of NCC better slightly than MCC, indicated by the increasing crystallinity index value from 74.8 to 76.4%, and it has a high thermal resistance of 330°C.

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Periodical:

Materials Science Forum (Volume 1057)

Pages:

11-18

DOI:

https://doi.org/10.4028/p-45x464

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Online since:

March 2022

Authors:

Ferriawan Yudhanto*, Harini Sosiati, Venditias Yudha, Edi Syafri

Keywords:

Acid Hydrolysis Process, Nanocrystalline Cellulose, Physical Characterization

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© 2022 Trans Tech Publications Ltd. All Rights Reserved

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