Hydrothermal Synthesis of Porous α-Fe2O3 Nanorods

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Porous α-Fe2O3 nanorods were successfully prepared by the hydrothermal method. The structure and morphology of the as-prepared α-Fe2O3 nanorods were characterized by powder X-ray diffracton (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and N2-sorption analysis. XRD studies ind icated that the as-prepared product was well-crystallized hematite phase of α-Fe2O3. The SEM and TEM images showed that the obtained α-Fe2O3 sample consisted of porous nanorods with the length of about 200 nm and diameter of about 50 nm. N2-sorption analysis indicated that the as-prepared sample possess mesoporous structure and high surface area (255.2 m2•g-1).

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195-199

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July 2011

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© 2011 Trans Tech Publications Ltd. All Rights Reserved

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[1] M.F. Haque, S. Arajs: Int. J. Heat Mass Transfer. Vol. 42(1999), pp.1617-1632.

Google Scholar

[2] Y. Einaga, M. Taguchi, G.M. Li et al.: Chem. Mater. Vol. 15(2003), pp.8-10.

Google Scholar

[3] D.N. Srivastava, N. Perkas, A. Gedanken et al.: J. Phys. Chem. B. Vol. 106(2002), pp.1878-1883.

Google Scholar

[4] Y.P. Zhang, Y. Chu, L.H. Dong: Nanotechnology Vol. 18(2007), p.435608.

Google Scholar

[5] D.S. Toledano, V.E. Henrich: J. Phys. Chem. B. Vol. 105(2001), pp.3872-3877.

Google Scholar

[6] Y. Wang, Y.M. Wang, J.L. Cao et al.: Sens. Actuators, B. Vol. 131(2008), pp.183-189.

Google Scholar

[7] Y. Wang, J.L. Cao, S.R. Wang et al.: J. Phys. Chem. C. Vol. 112(2008), pp.17804-17808.

Google Scholar

[8] J.L. Cao, Y. Wang, X.L. Yu et al.: Appl. Catal. B. Vol. 79(2008), pp.26-34.

Google Scholar

[9] U. Shwertmann, R.M. Cornell: Iron Oxides in the Laboratory, VCH, New York, (1991).

Google Scholar

[10] X.G. Peng, L. Manna, W.D. Yang et al.: Nature. Vol. 404(2000), pp.59-61.

Google Scholar

[11] Y. Qiu, D. Liu, J. Yang, S. Yang: Adv Mater Vol. 18(2006), pp.2604-2605.

Google Scholar

[12] N.N. Zhao, D.C. Pan, W. Nie, X.L. Ji: J. Am. Chem. Soc. Vol. 128(2006), pp.10118-10124.

Google Scholar

[13] D.D.D. Ma, C.S. Lee, F.C.K. Au et al.: Science. Vol. 299(2003), pp.1874-1877.

Google Scholar

[14] Z.H. Jing, S.H. Wu: Mater. Lett. Vol. 58(2004), pp.3637-3640.

Google Scholar

[15] D.D. Archibald, S. Mann: Nature. Vol. 364(1993), pp.430-433.

Google Scholar

[16] C.Z. Wu, P. Yin, X. Zhu et al.: J. Phys. Chem. B. Vol. 110(2006), pp.17806-17812.

Google Scholar