Sintering Sr2MgWO6 Ceramic and their Reactivity to Petroleum

Article Preview

Abstract:

This work has as main objectives to produce the ceramic Sr2MgWO6 and evaluate their reactivity to petroleum. Powders of SrCO3, MgO and WO3 were selected, taken in stoichiometric amounts and synthesized by conventional route. The synthesis was characterized by size distribution, specific surface area and thermogravimetric analysis (TGA). The synthesis was also fragmented into ball mill and characterized by specific surface. It was compacted, then was calcined at 1200 °C and analyzed by X-ray diffraction. The powders Sr2MgWO6 with perovskite structure were compacted and sintered at 1250, 1300 and 1350 °C. The materials produced were evaluated by microhardness, scanning electron microscopy (SEM), diffraction of X-rays and tests submersion in petroleum. The results showed that the ceramics have high microhardness and potential to be used in chemically aggressive environments such as petroleum.

You might also be interested in these eBooks

Info:

Periodical:

Materials Science Forum (Volumes 798-799)

Pages:

154-159

Citation:

Online since:

June 2014

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] H.M. Chandler: Ceramics in the Modern World: man's first technology comes of age. Aldus science and technology series, Aldus Books Inc., Menlo Park, Califórnia1968.

Google Scholar

[2] J.J. Reed: Principles of Ceramic Processing. (John Wiley and Sons New York, 1998).

Google Scholar

[3] D.W. Richardson: Modern Ceramic Engineering. (Marcel Dekker Inc. New York, 1982).

Google Scholar

[4] F.S. Galasso: Structure, Properties and Preparation of Perovskite Type Compounds. (Pergamon Press Inc. New York, 1969).

Google Scholar

[5] M. Marezio, J.P. Remeika and P.D. Dernier: Acta Crystallographica B Vol. 26 (1970).

Google Scholar

[6] Z.M. Fu, W.X. Li: Sci. Chin. Ser. A Vol. 38 (1995).

Google Scholar

[7] San-Dong Guo And Bang-Guiliu: Physica B Vol. 408 (2013), p.110.

Google Scholar

[8] B. Manoun, J.M. Igartua, P. Lazor: Journal of Molecular Structure Vol. 971 (2010), p.18.

Google Scholar

[9] S.N. Achary, K.R. Chakraborty, S.J. Patwe, A.B. Shinde, P.S.R. Krishna and A.K. Tyagi: Materials Research Bulletin Vol. 41 (2006), p.674.

DOI: 10.1016/j.materresbull.2005.07.025

Google Scholar