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HomeMaterials Science ForumMaterials Science Forum Vol. 852Microwave Synthesis of MOFs/Graphene Oxide...

Microwave Synthesis of MOFs/Graphene Oxide Composites and Hydrogen Storage Properties

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Abstract:

Metal-organic frameworks (MOFs: copper containing CuBTC)-graphene oxide (GO) composite (CG) was synthesized using microwave heating. The parent material and the composite were characterized by X-ray diffraction (XRD), thermogravimetric analysis (TGA), nitrogen sorption, scanning electron microscopy (SEM), high resolution transmission electron microscopy (HRTEM), Fourier transform infrared spectroscopy (HRTEM) and Raman spectroscopy. Then their hydrogen storage properties were systematically tested. The composite material CG shows a remarkable H₂capacity up to 2.43 wt% (28.6% increases vs. CuBTC) and higher surface area and pore volume compared to the neat CuBTC. And the particle size of CG is down to nanometer scale.

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Periodical:

Materials Science Forum (Volume 852)

Pages:

835-840

DOI:

https://doi.org/10.4028/www.scientific.net/MSF.852.835

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Online since:

April 2016

Authors:

Tian Bao Yang, Li Xian Sun, Fen Xu, Zi Qiang Wang

Keywords:

Graphene Oxide, Hydrogen Storage, Microwave, MOFs

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© 2016 Trans Tech Publications Ltd. All Rights Reserved

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