Papers by Author: Jason R. Jenny

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Abstract: Recent advances in PVT c-axis growth process have shown a path for eliminating micropipes in 4HN-SiC, leading to the demonstration of zero micropipe density 100 mm 4HN-SiC wafers. Combined techniques of KOH etching and cross-polarizer inspections were used to confirm the absence of micropipes. Crystal growth studies for 3-inch material with similar processes have demonstrated a 1c screw dislocation median density of 175 cm-2, compared to typical densities of 2x103 to 4x103 cm-2 in current production wafers. These values were obtained through optical scanning analyzer methods and verified by x-ray topography.
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Abstract: Micropipe density (MPD) is a crucial parameter for silicon carbide (SiC) substrates that determines the quality, stability and yield of the semiconductor devices built on these substrates. The importance of MPD is underscored by the fact that all existing specifications for 6H- and 4H-SiC substrates set upper limits for it. Several methods for measuring the MPD are known, however, their reliability and applicability to various types of substrates (e.g. semiinsulating, conducting, etc.) has not been systematically studied. The subject of this paper is a comparative study of various techniques used for the MPD measurement accompanied by statistical analysis of the results. The study was initiated by several organizations working in the immediate field of silicon carbide or in closely related fields and included SiC substrate manufacturers, substrate consumers, equipment manufacturers and universities. The study represented a round robin experiment in which MPD was measured on thirty SiC wafers of various pedigrees. The values of MPD have been determined using both destructive and non-destructive techniques. The repeatability of each technique is analyzed and compared with that of other techniques.
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Abstract: To devise a means of circumventing the cost of thick SiC epitaxy to generate drift layers in PiN diodes for >10kV operation, we have endeavored to enhance the minority carrier lifetimes in bulk-grown substrates. In this paper, we discuss the results of a process that has been developed to enhance minority carrier lifetimes to in excess of 30 μs in bulk-grown 4H-SiC substrates. Measurement of lifetimes was principally conducted using microwave-photoconductive decay (MPCD). Confirmation of the MPCD lifetime result was obtained by electron beam induced current (EBIC) measurements. Additionally, deep level transient spectroscopic analysis of samples subjected to this process suggests that a significant reduction of deep level defects in general and of Z1/Z2, specifically, may account for the significantly enhanced lifetimes. Finally, a study of operational performance in devices employing drift layers fabricated from substrates produced by this process confirmed ambipolar lifetimes in the microsecond range.
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