Preparation and Characterization of Nanometer Gallium Nitride by Gas-Solid Reaction

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Firstly, nano Gallium oxide(Ga2O3), as raw material of nano Gallium nitride(GaN), was prepared by special liquid-phase precipitation method. Subsequently,nano GaN powder was prepared by ammonia solution method through self-made experimental apparatus,and characterized by XRD and TEM methods. By controlling reaction temperature, reaction time and nitrogen flow,optimum parameters were determined to prepare nano GaN powder. Result shows that nano GaN powder, which is high purity and small particle, Can be prepared at 1000°C~1200°C holding above 2h and 100L/h flow

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97-102

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July 2015

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© 2015 Trans Tech Publications Ltd. All Rights Reserved

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