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Study on Synthesis Nanomicrostructures of Zinc Borate (Zn3B6O12•3.5H2O) with Different Morphologies

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Abstract:

The crystal zinc borate (Zn3B6O12·3.5H2O) nano-strips and nano-flakes were successfully prepared by a wet method using boric acid (H3BO3) and Zn(NO3)2·H2O as raw materials in situ aqueous solution, and triethanolamine as the modifying agent. The nano/microstructures and morphologies of the as-obtained samples were studied by X-ray diffraction (XRD), scanning electron microscopy (SEM) equipped with an energy dispersive X-ray spectrometer (EDS) and thermogravimetric analysis (TGA). It had been found that the as-prepared materials displayed nanostrips with average length from 100 to 200nm and the thicknesses about 30nm as well as nanoflakes with diameter about 4μm and thickness about several nanometers morphology.

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Periodical:

Advanced Materials Research (Volumes 236-238)

Pages:

1687-1691

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.236-238.1687

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Online since:

May 2011

Authors:

Hui Ren, You Ming Cao, Zhou Qiao Lei

Keywords:

Nano/Micro Structure, Zinc Borate

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© 2011 Trans Tech Publications Ltd. All Rights Reserved

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