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Preparation of Poly[4-Diacetoxyiodo] Styrene by Microwave Reactor

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Abstract:

The hypervalent organoiodine oxidant PDAIS( poly[4-diacetoxyiodo]styrene ) was prepared via the iodation and acetylation of polystyrene resin by microwave. Polystyrene was iodated with iodine/ iodine pentoxide in solvents such as nitrobenzene and tetrachloromethane, heating in microwave reactor could finish about 20min. The iodometery of loading capacity (ILC) of was up to 2.7mmol/g

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Advanced Materials Research II View Preview

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Periodical:

Advanced Materials Research (Volumes 463-464)

Pages:

523-526

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.463-464.523

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Online since:

February 2012

Authors:

Xiang Cheng Wang, Zhong Chao Dong, Xian Zhe Fu

Keywords:

Hypervalent Organoiodine Compounds, Microwave Reaction, Poly[4-diacetoxyiodo]styrene

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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