Effect of Thermal Treatment on the Texture and Structure of Sol-Gel Derived Carbon Nanotube/Silica Composites

Article Preview

Abstract:

The present work studies the structural and textural evolution of sol-gel derived carbon nanotube(CNT)/silica composites during the process of thermal treatment. The composites were prepared by sol-gel technique, and their structural and textural changes were traced by scanning electron microscopy, Raman spectra, infrared spectra, and thermogravimetric analysis. The results show that doped CNTs have an impact on the structural and textural evolution of CNT/silica composites during the process of thermal treatment and the CNT/silica composites exhibit good thermal stability during the heat treatment process. However, the composites are not densified even after treatment at 1000°C, quite different from the thermal behaviors of pure silica xerogel, due to the existing of guest CNTs.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

63-66

Citation:

Online since:

April 2013

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2013 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] R.D. Brooker, F.J. Guild, and A.C. Taylor: J. Mater. Sci. Vol. 46 (2011), p.3108.

Google Scholar

[2] M.P. Dash, M. Tripathy, A. Sasmal, G.C. Mohanty, and P.L. Nayak: J. Mater. Sci. Vol. 45 (2010), p.3858.

Google Scholar

[3] B. McCarthy, J.N. Coleman and R. Czerw: J. Phys. Chem. B Vol. 106 (2002), p.2210.

Google Scholar

[4] V.G. Gavalas, S.A. Law and J. Christopher Ball: Anal. Biochem. Vol. 329 (2004), p.247.

Google Scholar

[5] J.W. Ning, J.J. Zhang, Y.B. Pan and J.K. Guo: Mat. Sci. Eng. A-Struct. Vol. 357 (2003) p.392.

Google Scholar

[6] X.H. Chen, J.T. Xia and J.C. Peng: Compos. Sci. Technol. Vol. 602 (2000), p.301.

Google Scholar

[7] X.G. Wan, J.M. Dong and D.Y. Xing: Phys. Rev. B Vol. 58 (1998) p.6756.

Google Scholar

[8] K.C. Chin, A. Gohel, H.I. Elim, W.Z. Chen, W. Ji and G.L. Chong: J. Mater. Res. Vol. 21 (2006) p.2758.

Google Scholar

[9] A.M. Rao, A. Jorio, M.A. Pimenta, M.S.S. Dantas, R. Saito and G. Dresselhaus: Phys. Rev. Lett. Vol. 84 (2000) p.1820.

DOI: 10.1103/physrevlett.84.1820

Google Scholar

[10] Y. Zhang, Y. Shen, D. Han, Z. Wang, J. Song and Niu L. J. Mater. Chem. Vol. 16 (2006) p.4592.

Google Scholar

[11] S. Sakka: Handbook of Sol-gel Science and Technology, Processing, Characterization and Applications, VolumeⅡ, Characterization and Properties of Sol-gel Materials and Products (Kluwer Academic Publishers, New York 2005).

Google Scholar