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Determination of Pentachloronitrobenzene in Panax Ginseng by HPLC
Abstract:
The separation and determination of pentachloronitrobenzene powder within 10 min by HPLC with HP hypersil C18 column (4.6 mm × 250 mm), isocratic mobile phase of 0.05 mL/L disodium hydrogen phosphate and acetonitrile (35:65, v/v) containing 0.3 mL/L triethylamine at pH 6.2 and UV detector at 254 nm are described. The method is simple, rapid, sensitive and accurate. The intra-day and inter-day precision and accuracy, quantification limits and extraction yields are calculated for pentachloronitrobenzene at the sametime.
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516-519
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Online since:
December 2013
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© 2014 Trans Tech Publications Ltd. All Rights Reserved
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