Synthesis and Crystal Structure of Tridodecylammonium 3,5-Dinitro-1, 2, 4-1H-triazolate (TDADNT)

Tao Zhang; Long Liu; Yan Qiang Zhang; Zeng Xi Li

doi:10.4028/www.scientific.net/AMR.881-883.205

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 881-883Synthesis and Crystal Structure of...

Synthesis and Crystal Structure of Tridodecylammonium 3,5-Dinitro-1, 2, 4-1H-triazolate (TDADNT)

Abstract:

Tridodecylammonium 3,5-dinitro-1,2,4-1H-triazolate (TDADNT) was synthesized and characterized by NMR, IR, and Raman spectra, elemental analysis and TG/DTA. Its structure was further confirmed by the single crystal X-ray diffraction (Fig. 2), which shows that the compound crystallizes in the triclinic space group P-1 with a = 8.9507(19) Å, b = 12.702(2) Å, c = 19.068(4) Å, α = 72.440(5) ^o, β = 89.620(7) ^o, γ = 84.901(7) ^o, V = 2058.3(7) Å³, Z = 2. The salt is thermally stable up to 270 °C with the TG/DTA measurements.

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Advanced Materials Research (Volumes 881-883)

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205-210

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.881-883.205

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Online since:

January 2014

Authors:

Tao Zhang, Long Liu, Yan Qiang Zhang, Zeng Xi Li*

Keywords:

Crystal Structure, Thermal Decomposition, Tridodecylammonium 3,5-dinitro-1,2,4-1H-triazolate

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References

[1] V.M. Chernyshev, N.D. Zemlyakov, V.B. Il'in and V.A. Taranushich: Russ. J. Appl. Chem. Vol. 73 (2000), p.839.

Google Scholar

[2] K.Y. Lee, D.G. Ott and M.M. Stinecipher: Ind. Eng. Chem. Proc. Des. Dev. Vol. 20 (1981), p.358.

Google Scholar

[3] H. Xue, B. Twamley and J.M. Shreeve: J. Mater. Chem. Vol. 15 (2005), p.3459.

Google Scholar

[4] M. Smiglak, C.C. Hines, T.B. Wilson, S. Singh, A.S. Vincek, K. Kirichenko, A.R. Katritzky and R.D. Rogers: Chem. Eur. J. Vol. 16 (2010), p.1572.

DOI: 10.1002/chem.200901418

Google Scholar

[5] A.R. Katritzky, S. Singh, K. Kirichenko, J.D. Holbrey, M. Smiglak, W.M. Reichert and R.D. Rogers: Chem. Commun. (2005), p.868.

Google Scholar

[6] K.Y. Lee, D.G. Ott, L. Alamos and N. Mex, U.S. Patent 4, 236, 014. (1980).

Google Scholar

[7] K.Y. Lee, C.B. Storm, M.A. Hiskeyand and M.D. Coburn: J. Energ. Mater. Vol. 9 (1991), p.415.

Google Scholar

[8] R.L. Simpson, P.F. Pagoria, A.R. Mitchell and C.L. Coon: Propellants Explos. Pyrotech. Vol. 19 (1994), p.174.

DOI: 10.1002/prep.19940190405

Google Scholar

[9] Bruker, SHELXTL v2008/4. Bruker AXS Inc. Madison, (2008).

Google Scholar

[10] H.X. Gao, Z. Zeng, B. Twamley and J.M. Shreeve, Chem Eur. J. Vol. 14 (2008), p.1282.

Google Scholar

[11] L. He, G.H. Tao, D.A. Parrish and J.M. Shreeve: Chem. Eur. J. Vol. 16 (2010), p.5736.

Google Scholar