Preparation of C@ZrSiO4 Inclusion Pigment Using Compound Colorants via Non-Hydrolytic Sol-Gel Method

Xia Yi Xu; Wei Hui Jiang; Ting Chen; Jian Min Liu; Li Feng Miao; Xiao Jun Zhang

doi:10.4028/www.scientific.net/AMR.936.170

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 936Preparation of C@ZrSiO4 Inclusion Pigment Using...

Preparation of C@ZrSiO₄ Inclusion Pigment Using Compound Colorants via Non-Hydrolytic Sol-Gel Method

Abstract:

C@ZrSiO₄ inclusion pigment was prepared by using commercial carbon black RX8002C and phenolic resin (PF) as compound carbon source via non-hydrolytic sol-gel (NHSG) process. The RX8002C carbon could well disperse in phenolic resin solution, which developed a compound carbon source after calcination. Dense ZrSiO₄ layer was coated on the carbon surface as a protector. The structure and morphology of samples were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The chromatic value of the pigments was measured by the CIE color system. The results show that the compound colorants can be well coated by ZrSiO₄ dense layer to develop a black inclusion pigment. When the compound proportion is 1:4 and the compound colorants amount is 4wt.%, the chromatic value of the C@ZrSiO₄ inclusion pigment is 27.54.

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Advanced Materials Research (Volume 936)

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170-175

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.936.170

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Online since:

June 2014

Authors:

Xia Yi Xu, Wei Hui Jiang*, Ting Chen, Jian Min Liu, Li Feng Miao, Xiao Jun Zhang

Keywords:

C@ZrSiO₄ Inclusion Pigment, Compound Colorants, Non-Hydrolytic Sol-Gel Process

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References

[1] J. Calbo, S. Sorlí, M. Llusar, Minimization of toxicity in nickel ferrite black pigment, Bri. Ceram. Trans. 103(2004) 3-9.

DOI: 10.1179/096797804225012729

Google Scholar

[2] E. Ozel, S. Turan, Production of colored zirconium silicate pigments from zirconium silicate, J. Eur. Ceram. Soc. 27(2007) 1751-1757.

Google Scholar

[3] K.R. Pyon, B.H. Lee, The influence of firing conditions on the color properties of Pr-ZrSiO4 pigments synthesized using rice husk ash, J. Korean. Ceram. Soc. 46(2009) 397-404.

DOI: 10.4191/kcers.2009.46.4.397

Google Scholar

[4] Y. Zhang, D.Z. Zeng, P.G. Rao, Hydrothermal synthesis of cadmium sulfoselenide inclusion pigment, J. Sol-Gel. Sci. Technol. 48(2008) 289-293.

DOI: 10.1007/s10971-008-1838-5

Google Scholar

[5] M. Hosseini-Zori, F. Bondioli, T. Manfredini, Effect of synthesize parameters on a hematite-silica red pigment obtained using a coprecipitation route, Dyes. Pigments. 77(2008) 53-58.

DOI: 10.1016/j.dyepig.2007.03.006

Google Scholar

[6] F. Zhao, Y.F. Gao, H.G. Luo, Reactive formation of zirconium silicate inclusion pigments by deposition and subsequent annealing of a zirconium silicateia and silica double shell, Am. Chem. Soc. 23(2009) 13295-13297.

DOI: 10.1021/la903197t

Google Scholar

[7] R. Corriu, P.H. Mutin, D. Leclercq, Preparation of monolithic metal oxide gels by a non-hydrolytic sol-gel process, J. Mater. Chem. 2(1992) 673-674.

DOI: 10.1039/jm9920200673

Google Scholar

[8] W.H. Jiang, Y.H. Yang, Q.X. Zhu, Iron-zirconium silicate pigments prepared by non-hydrolytic sol-gel method at low temperature, Adv. Mater. Res. 412(2012) 223-226.

DOI: 10.4028/www.scientific.net/amr.412.223

Google Scholar

[9] W.H. Jiang, Y. Feng, J.M. Liu, Preparation of ZrSiO4/C Inclusion pigments by non-hydrolytic sol-gel method combined with the process of carbon black modification, Mater. Sci. Forum. 745(2013) 545-550.

DOI: 10.4028/www.scientific.net/msf.745-746.545

Google Scholar

[10] F. Zhao, W.D. Li, H.J. Luo, Sol-gel modified method for obtention of gray and pink ceramic pigments in zircon matrix, J. Sol-Gel Sci. Technol. 49 (2009) 247-252.

DOI: 10.1007/s10971-008-1864-3

Google Scholar

[11] Z.Y. Jiang, S.Q. Li, J.M. Zeng, Preparation and characterization of self-dispersal nanometer carbon black pigment, Adv. Mater. Res. 189(2011) 3836-3839.

DOI: 10.4028/www.scientific.net/amr.189-193.3836

Google Scholar

[12] H Zhao, M Deng, Effects of the synthetic ways of sulfonated-phenol-formaldehyde (SPF) polymers on application properties of cementitious materials, Polym-Plast. Technol. 50(2011) 916-922.

DOI: 10.1080/03602559.2011.551983

Google Scholar

[13] S Kongwudthiti, P Praserthdam, W Tanakulrrungsank, M Inoue, The influence of Si–O–Zr bonds on the crystal-growth inhibition of zirconium silicateia prepared by the glycothermal method, J. Mater. Process. Technol. 136(2003) 186-189.

DOI: 10.1016/s0924-0136(03)00157-2

Google Scholar

[14] XJ Yang, MZ Qiu, LQ Hu, B Wu, Effects of nanometer carbon powder on the ablative and heat protection properties of phenolic resin (In Chinese), Journal of solid rocket technology. 27(2004) 2.

Google Scholar