Properties of Cryogenic Treated Cemented Carbides (WC-Co)

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The present paper explores the effects of deep cryogenic treatment (DCT) on the properties of WC-Co cemented carbides. The investigation involved four different cemented carbide (CC) grades. Two of them were coarse-grained WC with grain sizes larger than 6 μm and binder fractions of 10 and 15 wt. %. The other two were fine-grained with WC grains of 0.5-0.8 μm and the same binder fractions of 10 and 15 wt. %. Their specimens were ground and polished to prepare them for DCT. In each specimen, one half of this polished surface was used for testing the properties of the CC before cryogenic treatment. The post-DCT properties were then determined on the other half. Properties of the cemented carbides prior to and after DCT were studied using optical and scanning electron microscopy, X-ray diffraction, hardness testing according to Vickers scale followed by calculation of fracture toughness KIC and a ball-on-disk test of the wear resistance of the surface. One of the findings was that cryogenic treatment led to a decrease in residual stresses and to lower fracture toughness KIC in the CC.

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September 2020

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[1] Bryson, W. E.: Cryogenics. Hanser Gardner Publications, Cincinnati, USA, (1999).

Google Scholar

[2] Hájek, J. a kol., Kryogenní zpracování brzdových kotoučů [online]. 2018 [cit. 2019-02-28]. Available at:https://www.autodilycardo.cz/db/downloads/38_Kryogenni_zpracovani_ brzdovych_kotoucu_eci.pdf.

Google Scholar

[3] Kříž, A., Hájek, J., Chocholatý, O., Průcha, V. Effect of deep cryogenic treatment on properties of aluminium bronze. In European Conference on Heat Treatment 2016. 2016. ISBN: 978-80-904462-9-8.

Google Scholar

[4] Carlson, E. Cold treating and cryogenic treatment of steel. ASM International, ASM Handbook.1991, 4: 203-206.

Google Scholar

[5] Nižňanská, J.: Vliv kryogenního zpracování na vlastnosti nástrojových ocelí pro práci za tepla, diploma thesis. Department of Material Science and Technology, Faculty of Mechanical Engineering, University of West Bohemia, (2014).

Google Scholar

[6] Huang, J. Y., et al. Microstructure of cryogenic treated M2 tool steel. Materials Science and Engineering: A, 2003, 339.1-2: 241-244.

DOI: 10.1016/s0921-5093(02)00165-x

Google Scholar

[7] Stratton, P.F.: In.: Proc. of the 1st Int. Conf. on Heat Treatment and Surf. Engng. of Tools and Dies, Pula, Croatia, 8.-11.6.2005,11.

Google Scholar

[8] Vadilek, K. and R. Rudramoorthy. Performance analysis of cryogenically treated coated carbide inserts. The International Journal of Advanced Manufacturing Technology [online]. 2009, 42(3-4), 222-232 [cit. 2020-01-30].

DOI: 10.1007/s00170-008-1597-z

Google Scholar

[9] Gill, Simranpreet Singh, Harpreet Singh, Rupinder Singh a Jagdev Singh. Flank Wear and Machining Performance of Cryogenically Treated Tungsten Carbide Inserts. Materials and Manufacturing Processes [online]. 2011, 26(11), 1430-1441 [cit. 2020-01-30].

DOI: 10.1080/10426914.2011.557128

Google Scholar

[10] Yong, Jiang a Chen Ding. Effect of cryogenic treatment on WC–Co cemented carbides. Materials Science and Engineering: A [online]. 2011, 528(3), 1735-1739 [cit. 2020-01-30].

DOI: 10.1016/j.msea.2010.11.009

Google Scholar

[11] Yong, A.Y.L., K.H.W. Seah a M. Rahman. Performance evaluation of cryogenically treated tungsten carbide tools in turning. International Journal of Machine Tools and Manufacture [online]. 2006, 46(15), 2051-2056 [cit. 2020-01-30].

DOI: 10.1016/j.ijmachtools.2006.01.002

Google Scholar

[12] Kalsi, N.S., Sehgal, R. & Sharma, V.S. Effect of tempering after cryogenic treatment of tungsten carbide–cobalt bounded inserts. Bull Mater Sci 37, 327–335 (2014). Available at: https://doi.org/10.1007/s12034-014-0634-9.

DOI: 10.1007/s12034-014-0634-9

Google Scholar

[13] Editor-in-chief Vinod K. Sarin a Luis Lanes edited by Daniele Mari. (2014). Comprehensive hard materials, Volume 1, Hardmetals. Elsevier.ISBN 9780080965284.

Google Scholar

[14] Yong, A. Y. L., K. H. W. Seah a M. Rahman. Performance of cryogenically treated tungsten carbide tools in milling operations. The International Journal of Advanced Manufacturing Technology [online]. 2007, 32(7-8), 638-643 [cit. 2020-01-31].

DOI: 10.1007/s00170-005-0379-0

Google Scholar

[15] Akincioglu, Sıtkı, Hasan Gokkaya and İlyas Uygur. A review of cryogenic treatment on cutting tools. The International Journal of Advanced Manufacturing Technology [online]. 2015, 78(9-12), 1609-1627 [cit. 2020-01-31].

DOI: 10.1007/s00170-014-6755-x

Google Scholar

[16] Ruperinder, s. Enhancement of Tool Material Machining Characteristics with Cryogenic Treatment: A Review. Proceedings of the 2010 International Conference on Industrial Engineering and Operations Management Dhaka, Bangladesh, January 9-10, 2010. Available at: http://www.iieom.org/paper/Final%20Paper%20for%20PDF/164%20Rupinder%20Singh%20Khalsa.pdf.

Google Scholar

[17] Padmakumar, M., D. Dinakaran and J. Guruprasath. Characterization of cryogenically treated cemented carbide. Integrated Ferroelectrics [online]. 2017, 185(1), 65-72 [cit. 2020-01-31].

DOI: 10.1080/10584587.2017.1370340

Google Scholar

[18] Ishida, K and T Nishizawa. The C-Co (Carbon-Cobalt) system. Journal of Phase Equilibria [online]. 1991, 12(4), 417-424 [cit. 2020-01-31].

DOI: 10.1007/bf02645959

Google Scholar

[19] Thakur, Dinesh, B. Ramamoorthy and L. Vijayaraghavan. Influence of different post treatments on tungsten carbide–cobalt inserts. Materials Letters [online]. 2008, 62(28), 4403-4406 [cit. 2020-02-03].

DOI: 10.1016/j.matlet.2008.07.043

Google Scholar

[20] Zhang, Hejia, Liqing Chen, Jing Sun, Wenguang Wang a Quanzhao Wang. An investigation of cobalt phase structure in WC–Co cemented carbides before and after deep cryogenic treatment. International Journal of Refractory Metals and Hard Materials [online]. 2015, 51, 201-206 [cit. 2020-02-03].

DOI: 10.1016/j.ijrmhm.2015.04.007

Google Scholar

[21] Wear parts – a complete catalogue [online]. CERATIZIT S.A., 2015 [cit. 2020-01-30]. Available at: https://www.ceratizit.com/uploads/tx_extproduct//files/GD_KT_PRO-0272-0915_SCS_ABS_V1.pdf.

Google Scholar

[22] ASTM B 657-92 Standard Guide for Metallographic Identification of Microstructure in Cemented Carbides. [online] Astm.org. Available at: https://www.astm.org/Standards/B657.htm [Accessed 2 Apr. 2019].

Google Scholar

[23] ISO 4499-1, Hardmetals — Metallographic determination of microstructure — Part 4: Characterisation of porosity, carbon defects and eta-phase content.

DOI: 10.3403/30275876u

Google Scholar

[24] ASTM G99 2016 Standard Test Method for Wear Testing with a Pin-on-Disk Apparatus. [online] Astm.org. Available at: https://www.astm.org/ DATABASE.CART/HISTORICAL/G99-05R16.htm [Accessed 28 Aug. 2019].

Google Scholar

[25] ISO 3878: 1983 Hardmetals — Vickers Hardness. Geneva, Switzerland, (1983).

Google Scholar

[26] ISO 28079: 2009 Hardmetals — Palmqvist Toughness. Geneva, Switzerland, (2009).

Google Scholar