Preparation, Microstructure and Properties of Ti-6Al-4V Rods by Powder Compact Extrusion of TiH2/Al60V40 Powder Mixture

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Ti-6Al-4V (wt.%) alloy rods were prepared successfully using a low-cost and short powder metallurgy process that involves mixing TiH2 and Al60V40 powders, compacting the powder blend and extruding the powder compact at elevated temperatures. The microstructure and mechanical properties of Ti-6Al-4V alloy and the effects of particle size, oxygen content and heat treatment on them were investigated. The results showed that the microstructure and homogeneity of the extruded rods were strongly affected by the particle size of TiH2/Al60V40 powder blends. By changing tumbler mixing into low-energy ball milling, the TiH2/Al60V40 particle sizes decreased, and the volume fraction of undissolved V rich particles in the microstructure of the extruded rod substantially decreased from 8.6% to zero. High yield strength and ultimate tensile strength of 1154 and 1353 MPa respectively with a moderate elongation to fracture of 3.6% are achieved with the Ti-6Al-4V rod prepared by using the powder blend. The extruded Ti-6Al-4V rod prepared using the ball milled powder had a very high strength, but limited ductility due to a high oxygen content. Solution treatment and aging slightly increase the strength of Ti-6Al-4V rods at the cost of dramatic decrease of ductility.

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116-125

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May 2018

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© 2018 Trans Tech Publications Ltd. All Rights Reserved

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[1] C. Cui, B. Hu, L. Zhao, S. Liu, Titanium alloy production technology, market prospects and industry development, Mater Design, 32(3) (2011) 1684-1691.

DOI: 10.1016/j.matdes.2010.09.011

Google Scholar

[2] G. Welsch, R. Boyer, E. Collings, Materials properties handbook: titanium alloys, first ed., ASM international, USA, (1993).

Google Scholar

[3] F. Yang, D.L. Zhang, H.Y. Lu, B. Gabbitas, Preparation, microstructure and properties of Ti-6Al-4V rods by powder compact extrusion of powder mixture, Key Eng. Mater., 520 (2012) 70-75.

DOI: 10.4028/www.scientific.net/kem.520.70

Google Scholar

[4] F. Cao, K.R. Chandran, P. Kumar, New approach to achieve high strength powder metallurgy Ti-6Al-4V alloy through accelerated sintering at β-transus temperature and hydrogenation-dehydrogenation treatment, Scripta Mater., 130 (2017) 22-26.

DOI: 10.1016/j.scriptamat.2016.11.005

Google Scholar

[5] J.D. Paramore, Z.Z. Fang, P. Sun, M. Koopman, K.R. Chandran, M. Dunstan, A powder metallurgy method for manufacturing Ti-6Al-4V with wrought-like microstructures and mechanical properties via hydrogen sintering and phase transformation (HSPT), Scripta Mater., 107 (2015).

DOI: 10.1016/j.scriptamat.2015.05.032

Google Scholar

[6] F. Cao, K.R. Chandran, P. Kumar, P. Sun, Z.Z. Fang, M. Koopman, New powder metallurgical approach to achieve high fatigue strength in Ti-6Al-4V alloy, Metal. Mater. Trans. A, 47(5) (2016) 2335-2345.

DOI: 10.1007/s11661-016-3409-7

Google Scholar

[7] O.M. Ivasishin, V.M. Anokhin, A.N. Demidik, D.G. Savvakin, Cost-Effective Blended Elemental Powder Metallurgy of Titanium Alloys for Transportation Application, Key Eng. Mater., 188 (2000) 55-62.

DOI: 10.4028/www.scientific.net/kem.188.55

Google Scholar

[8] L. Xiao, W. Lu, Z. Yang, J. Qin, D. Zhang, M. Wang, F. Zhu, B. Ji, Effect of reinforcements on high temperature mechanical properties of in situ synthesized titanium matrix composites, Mat Sci Eng A-Struct, 491(1) (2008) 192-198.

DOI: 10.1016/j.msea.2008.01.077

Google Scholar

[9] L. Huang, L. Geng, B. Wang, H. Xu, B. Kaveendran, Effects of extrusion and heat treatment on the microstructure and tensile properties of in situ TiBw/Ti6Al4V composite with a network architecture, Compos Part A-Appl S, 43(3) (2012) 486-491.

DOI: 10.1016/j.compositesa.2011.11.014

Google Scholar

[10] D.J. McEldowney, S. Tamirisakandala, D.B. Miracle, Heat-treatment effects on the microstructure and tensile properties of powder metallurgy Ti-6Al-4V alloys modified with boron, Metal. Mater. Trans. A, 41A(4) (2010) 1003-1015.

DOI: 10.1007/s11661-009-0157-y

Google Scholar

[11] Y. Zheng, X. Yao, J. Liang, D. Zhang, Microstructures and tensile mechanical properties of titanium rods made by powder compact extrusion of a titanium hydride powder, Metal. Mater. Trans. A, 47(4) (2016) 1842-1853.

DOI: 10.1007/s11661-016-3333-x

Google Scholar

[12] Z. Zhang, S. Qu, A. Feng, J. Shen, D. Chen, Hot deformation behavior of Ti-6Al-4V alloy: Effect of initial microstructure, J. Alloys Compd, 718 (2017) 170-181.

DOI: 10.1016/j.jallcom.2017.05.097

Google Scholar

[13] C. Azevedo, D. Rodrigues, F.B. Neto, Ti-Al-V powder metallurgy (PM) via the hydrogenation-dehydrogenation (HDH) process, J. Alloys Compd, 353(1) (2003) 217-227.

DOI: 10.1016/s0925-8388(02)01297-5

Google Scholar

[14] S. Zherebtsov, M. Murzinova, G. Salishchev, S. Semiatin, Spheroidization of the lamellar microstructure in Ti-6Al-4V alloy during warm deformation and annealing, Acta Mater., 59(10) (2011) 4138-4150.

DOI: 10.1016/j.actamat.2011.03.037

Google Scholar

[15] Y. Zheng, X. Yao, Y. Su, D. Zhang, High strength titanium with a bimodal microstructure fabricated by thermomechanical consolidation of a nanocrystalline TiH2 powder, Mat Sci Eng A-Struct, 686 (2017) 11-18.

DOI: 10.1016/j.msea.2017.01.029

Google Scholar

[16] T. Takahashi, Y. Minamino, M. Komatsu, Interdiffusion in β Phase of the Ternary Ti-Al-V System, Mater. Trans, 49(1) (2008) 125-132.

DOI: 10.2320/matertrans.mra2007110

Google Scholar

[17] T. Ahmed, H. Rack, Phase transformations during cooling in α+ β titanium alloys, Mat Sci Eng A-Struct, 243(1) (1998) 206-211.

Google Scholar

[18] F. Yang, B. Gabbitas, Effect of heat treatment on microstructures and mechanical properties of a Ti-6Al-4V alloy rod prepared by powder compact extrusion, Int. J. Mod Phys B, 29 (2015) 1-7.

DOI: 10.1142/s0217979215400044

Google Scholar