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HomeKey Engineering MaterialsKey Engineering Materials Vol. 822Effect of the Mechanical Alloying and Spark Plasma...

Effect of the Mechanical Alloying and Spark Plasma Sintering on Microstructure, Phase Composition and Chemical Elements Distribution of Nb-Si Based Composite

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Abstract:

Synthesis of the Nb-Si in-situ composite was attempted by mechanical alloying of element powders in vario-planetary ball mill. The particles size distribution was measured by laser diffraction, microstructures were examined with scanning electronic microscope, and the phase constituent were analyzed by X-ray diffraction. The amorphization of the Si during mechanical alloying, large amount of deformation of Nb crystal structure, and after all – the formation of supersaturated solid solution of Nb was observed. To stabilize microstructure and phase composition, a spark plasma sintering was attempted. After SPS microstructure consist of three main phases – Nb_ss, Nb₅Si₃ and Nb₃Si.

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Periodical:

Key Engineering Materials (Volume 822)

Pages:

617-627

DOI:

https://doi.org/10.4028/www.scientific.net/KEM.822.617

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Online since:

September 2019

Authors:

I.S. Goncharov*, Nikolay Razumov, Aleksey I. Shamshurin, Qing Sheng Wang

Keywords:

In-Situ Composites, Mechanical Alloying, Nb-Si, Spark Plasma Sintering

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© 2019 Trans Tech Publications Ltd. All Rights Reserved

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