Materials Science Forum Vols. 702-703

Abstract: The evolution of microstructure and texture in Hexagonal Close Pack commercially pure titanium has been studied in torsion in a strain rate regime of 0.001 to 1 s-1. Free end torsion tests carried out on titanium rods indicated higher stress levels at higher strain rate but negligible change in the strain-hardening behaviour. There was a decrease in the intra-granular misorientation while a negligible change in the amount of contraction and extension twins was observed with increase in strain rate. The deformed samples showed a C1 fibre (c-axis is first rotated 90° in shear direction and then +30° in shear plane direction) at all the strain rates. With the increase in strain rate, there was an increase in the intensity of the C1 fibre and it became more heterogeneous with a strong {11 6} component. In the absence of extensive twinning, pyramidal slip system is attributed for the observed deformation texture. The present investigation, therefore, substantiates the theoretical prediction of increase in strength of texture with strain rate in torsion.

Abstract: In this study a systematic characterization of the microstructural and textural evolution in each thermo-mechanical processing step of Zircaloy-4 rod fabrication has been carried out. The possible micro-mechanisms leading to the observed microstructural evolutions have been discussed. The thermo-mechanical steps followed resulted in a completely recrystallized microstructure and retention of the hot-extruded texture in the finished product.

Abstract: The mechanical behaviour and texture evolution during uniaxial compression of Zircaloy-4 at different temperatures (25, 300, 500 C) has been studied. At room temperature and 300 C the texture evolution and strain-hardening behaviour observed are attributed to the activation of {10-12} tensile twinning, which can be identified in optical micrographs and electron backscatter diffraction (EBSD) data. The influence of twinning upon the texture evolution and hardening rate becomes less apparent with increasing temperature. Nevertheless twinning is still active at 500 C. Simulation of the texture evolution at 500 C using crystal plasticity finite element modelling (CPFEM) indicates that slip alone cannot explain the experimentally observed textures at this temperature.

Abstract: The present study deals with deformation behaviour of textured Zircaloy 2 with two dominant orientations: basal and non-basal. During initial stages (20%), two distinct class of grains were observed – non-deforming/non-fragmenting grains and deforming/fragmenting grains. The so-called non- deforming/non-fragmenting grains remain equiaxed even after 50% of deformation. They also have insignificant in-grain misorientation developments and have more residual stresses. Dislocation dynamics simulation showed that the dislocation interactions/mobility is insignificant in basal orientations at room temperature deformations.

Abstract: Features of the deformation process by cold radial forging of tube billets from Zr-1%Nb alloy were reconstructed on the basis of X-ray texture data. The cold radial forging intensifies grain fragmentation in the bulk of billet and increases significantly the latent hardening of potentially active slip systems, so that operation only of the single slip system becomes possible. As a result, in radially-forged billets unusual deformation and recrystallization textures arise, differing from usual textures of a-Zr by the mutual inversion of crystallographic axes, aligned along the axis of tube.

Abstract: In this contribution, we describe the basic principles to reconstruct parent microtextures from inherited ones. The different methods published in the literature are examined. Their various approaches lead to different restitution capabilities and we discuss their advantages and weaknesses.

Abstract: There has recently been significant interest in the problem of variant selection in the strain-induced transformation of austenite to α’-martensite in metastable austenitic stainless steels. Previous work has highlighted our poor understanding of the mechanisms leading to this transformation, in particular the role that the macroscopic stress plays in the transformation. In this work, we have sought to perform detailed experiments aimed at developing a statistical grain level view of variant selection in one particular grade of austenitic stainless steel. EBSD measurements made over a large number of grains as well as macroscopic texture measurements made at different levels of imposed plastic strain allow for comparison against various approaches for predicting variant selection based on the Patel-Cohen interaction energy.

Abstract: In the present study, in situ phase transformation experiments have been carried out using neutron diffraction to monitor the texture evolution during the α→ß→α phase transformation in Ti-6Al-4V with and without 0.4% yttrium additions. The aim of adding yttrium was to control ß grain growth above the transus ß by grain boundary pinning. In the present case, strengthening of the ß texture, occurring during ß grain coarsening resulted in strengthening of particular ß texture components, which increases the likelihood of α texture modification by selective growth of α variants on the common (110) ß grain boundaries into unoccupied large β grains.

Abstract: A nanostructured surface layer was synthesized in a pure copper plate by means of surface mechanical attrition (SMA). The evolutions of microstructure and orientation were examined by using XRD, TEM and ODF. The microstructural evolution with the treatment time can be divided into two stages: the first is characterized by a formation of nc grains with small to medium misorientations in the surface layer and a texture transformation from rolling type to shear one in the near-surface layer, and the second by a significant increment of misorientations between the nc grains and a texture transformation from shear type back to rolling one. It might be reasonably deduced that shear stress can effectively induce grain refinement, and the combination of shear and compress stresses might be helpful for the increment of grain boundary misorientations.

Abstract: In this contribution, we investigate a method able to determine the local representative orientation relation occurring in phase transformation of steels. It is based on the analysis of sets of variant orientations and does not require the knowledge the parent austenite orientation. The method which is an optimization scheme employing quaternions allowed us to determine and investigate ORs of different low carbon steel products.