Microstructure Evolution of Hybrid TiO2 Nanowire-Nanotube Structure Fabricated by Anodization

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Hybrid TiO2 nanowire–nanotube structure was synthesized by a facile anodization on Ti substrate. To study the origin and evolution of TiO2 nanotubes, the morphology of TiO2 nanotubes was investigated. It was found that nanotubes corrode gradually into nanowires, and the critical time was about 8.5 h after the beginning of anodization. Uniform nanotubes were obtained by ultrasonic cleaning. It was demonstrated experimentally that the inner diameter of TiO2 nanotube increased with the extension of anodization time, but the outer diameter of TiO2 nanotubes, which were fabricated under different anodization time, was almost the same.

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428-432

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April 2016

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© 2016 Trans Tech Publications Ltd. All Rights Reserved

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