Influence of Starting Microstructure on Dilatation Behavior during Tempering of a High Strength Steel

Article Preview

Abstract:

The aim of this study was to determine the effect of non-isothermal tempering on microstructure evolution in large-size slabs. Using high-resolution dilatometry, three different cooling rates (from 0.08 to 3°C/s) representative of different regions from the surface to the core of the slab were experimentally simulated, and then tempering was carried out for each starting microstructure. A combination of light and electron microscopy and X-ray diffraction analyses were employed to accurately analyze different phenomena occurring during the tempering process, specially, the identification of different microstructures (bainite, martensite and retained austenite), and the determination of the percentage of retained austenite for each experimental condition were considered. Experimental results revealed that the microstructure after the cooling rate of 0.08°C/s consisted of bainite and some retained austenite. For the cooling rate of 0.3°C/s, martensite plus bainite was detected, and when the cooling rate was increased to 3°C/s, a martensitic microstructure was obtained. Analysis of dilatometry curves indicated that tempering behavior varied significantly with the starting microstructure. Martensite tempering was accompanied with a length decrease due to the decomposition of medium-carbon martensite to low-carbon martensite plus carbides. Tempering of bainite and retained austenite resulted in a remarkable length increase.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

305-310

Citation:

Online since:

December 2018

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2018 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] Liu, D.; Wang, G.; Liu, X.; Zhao, D. Effect of cooling rates and compressive deformation of austenite on bainitic transformation and microstructure for plastic die aisi p.20 steel. ISIJ International, 38 (1998) 482-488.

DOI: 10.2355/isijinternational.38.482

Google Scholar

[2] Chentouf, S.M.; Jahazi, M.; Lapierre-Boire, L.-P.; Godin, S. Characteristics of austenite transformation during post forge cooling of large-size high strength steel ingots. Metallography, Microstructure, and Analysis, 3 (2014) 281-297.

DOI: 10.1007/s13632-014-0142-8

Google Scholar

[3] Wu, R.M.; Zheng, Y.F.; Wu, X.C.; Li, X.C. Effect of titanium on the microstructure and hardness uniformity of non-quenched and tempered prehardened steel for large-section plastic mould. Ironmaking & Steelmaking, 44 (2017) 17-22.

DOI: 10.1080/03019233.2016.1155830

Google Scholar

[4] Speich, G.R.; Leslie, W.C. Tempering of steel. Metallurgical Transactions, 3 (1972) 1043-1054.

DOI: 10.1007/bf02642436

Google Scholar

[5] Morra, P.V.; Böttger, A.J.; Mittemeijer, E.J. Decomposition of iron-based martensite. A kinetic analysis by means of differential scanning calorimetry and dilatometry. Journal of Thermal Analysis and Calorimetry, 64 (2001) 905-914.

DOI: 10.1023/a:1011514727891

Google Scholar

[6] Yan, G.; Han, L.; Li, C.; Luo, X.; Gu, J. Characteristic of retained austenite decomposition during tempering and its effect on impact toughness in sa508 gr.3 steel. Journal of Nuclear Materials, 483 (2017) 167-175.

DOI: 10.1016/j.jnucmat.2016.11.011

Google Scholar

[7] Cheng, L.; Brakman, C.M.; Korevaar, B.M.; Mittemeijer, E.J. The tempering of iron- carbon martensite; dilatometric and calorimetric analysis. Metallurgical Transactions A, 19 (1988), 2415-2426.

DOI: 10.1007/bf02645469

Google Scholar

[8] Nagakura, S.; Hirotsu, Y.; Kusunoki, M.; Suzuki, T.; Nakamura, Y. Crystallographic study of the tempering of martensitic carbon steel by electron microscopy and diffraction. Metallurgical Transactions A, 14 (1983)1025-1031.

DOI: 10.1007/bf02670441

Google Scholar

[9] Primig, S.; Leitner, H. Separation of overlapping retained austenite decomposition and cementite precipitation reactions during tempering of martensitic steel by means of thermal analysis. Thermochimica Acta, 526 (2011) 111-117.

DOI: 10.1016/j.tca.2011.09.001

Google Scholar

[10] Miller, M.K.; Beaven, P.A.; Smith, G.D.W. A study of the early stages of tempering of iron-carbon martensites by atom probe field ion microscopy. Metallurgical Transactions A, 12 (1981) 1197-1204.

DOI: 10.1007/bf02642333

Google Scholar

[11] Talebi, S.; Ghasemi-Nanesa, H.; Jahazi, M.; Melkonyan, H. In situ study of phase transformations during non-isothermal tempering of bainitic and martensitic microstructures. Metals, 7 (2017) 346.

DOI: 10.3390/met7090346

Google Scholar

[12] Nahamin Pardazan Asia, MIP (Metallographical Image Processing) (2018), Iran, (http://en.metsofts.ir).

Google Scholar

[13] Liu, F.; Lin, X.; Song, M.; Yang, H.; Song, K.; Guo, P.; Huang, W. Effect of tempering temperature on microstructure and mechanical properties of laser solid formed 300m steel. Journal of Alloys and Compounds, 689 (2016) 225-232.

DOI: 10.1016/j.jallcom.2016.07.276

Google Scholar