Synthesis of Mesoporous Nickel Phosphate with Long Hollow Nanotubes

Juan Tan; Xu Ying Li; Fei Yang; Jing Liu

doi:10.4028/www.scientific.net/AMR.399-401.625

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 399-401Synthesis of Mesoporous Nickel Phosphate with Long...

Synthesis of Mesoporous Nickel Phosphate with Long Hollow Nanotubes

Abstract:

Mesostructured nickel phosphate was synthesized with urea as alkali by sol-gel method. The obtained material nominated as NiPO-3 was characterized by means of XRD, ICP, FT-IR, TEM, and N₂ adsorption. In contrast to mesoporous nickel phosphate NiPO-1 and NiPO-2 we reported before, NiPO-3 exhibits relatively longer nanotubes reached up to 400~600 nm. N2 adsorption shows that NiPO-3 possesses high BET surface area (345.8 m²g^-1) and pore volume (0.46 cm³g^-1). The catalytic performance of NiPO-3 showed that the total selectivity of epoxycyclohexane and hexadienol was as high as 83.38%.

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Periodical:

Advanced Materials Research (Volumes 399-401)

Pages:

625-628

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.399-401.625

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Online since:

November 2011

Authors:

Juan Tan, Xu Ying Li, Fei Yang, Jing Liu

Keywords:

Cetyl Trimethyl Ammonium Bromide (CTAB), Mesoporous, Nanotube, Nickel Phosphate, NiPO, Sol-Gel (SG)

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