Preparation of Magnetic Fe3O4 Nanoparticles by Microbial Reduction Combining Natural Oxidation Method

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Abstract:

By using microbial reduction combining natural oxidation method, magnetic Fe3O4 nanoparticles have been synthesized. Sulfate-reducing bacterium(SRB) was used to reduce ferric sulfate to produce ferric sulfide, then ferric sulfide was oxidized to iron protoxide and ferroferric oxide in the end under natural air oxidation condition. The size and morphology of the product and SRB was examined by scanning electron microscopy(SEM), the microstructure were investigated by X-ray diffraction(XRD) and energy dispersive spectroscopy(EDS). There are only two components(xFeO and yFe3O4)which is testified by XRD and EDS. The constituents of product were analysed by using energy dispersive spectroscopy(EDS). In result, x,y actual numerical value which is respectively mole fraction of FeO and Fe3O4 in the product is figured out 0.678 and 0.322.

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Advanced Materials Research (Volumes 399-401)

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949-953

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November 2011

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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